BMRB Entry 25925

Title:
Chemical shift assignments of rv3053c from Mycobacterium tuberculosis in the oxidized state
Deposition date:
2015-12-18
Original release date:
2016-01-12
Authors:
Feng, Yingang
Citation:

Citation: Liu, Ya-Jun; Song, Xiaxia; Li, Yifei; Xuan, Jinsong; Cui, Qiu; Wang, Jinfeng; Feng, Yingang. "Low stability of the reduced state of Mycobacterium tuberculosis NrdH redoxin"  FEBS Lett. 590, 387-395 (2016).
PubMed: 26786191

Assembly members:

Assembly members:
rv3053c, polymer, 87 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: Mycobacterium tuberculosis   Taxonomy ID: 1773   Superkingdom: Bacteria   Kingdom: not available   Genus/species: Mycobacterium tuberculosis

Experimental source:

Experimental source:   Production method: recombinant technology   Host organism: Escherichia coli   Vector: pET30a

Entity Sequences (FASTA):

Data sets:
Data typeCount
13C chemical shifts360
15N chemical shifts88
1H chemical shifts571

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1rv3053c1

Entities:

Entity 1, rv3053c 87 residues - Formula weight is not available

1   METTHRVALTHRVALTYRTHRLYSPROALA
2   CYSVALGLNCYSSERALATHRSERLYSALA
3   LEUASPLYSGLNGLYILEALATYRGLNLYS
4   VALASPILESERLEUASPSERGLUALAARG
5   ASPTYRVALMETALALEUGLYTYRLEUGLN
6   ALAPROVALVALVALALAGLYASNASPHIS
7   TRPSERGLYPHEARGPROASPARGILELYS
8   ALALEUALAGLYALAALALEUTHRALALEU
9   GLUHISHISHISHISHISHIS

Samples:

sample_1: rv3053c, [U-13C; U-15N], 1.0 mM; potassium phosphate 50 mM; potassium chloride 100 mM; DSS 0.02 % w/v

sample_conditions_1: ionic strength: 150 mM; pH: 6; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-15N HSQCsample_1isotropicsample_conditions_1
2D 1H-13C HSQCsample_1isotropicsample_conditions_1
3D HNCOsample_1isotropicsample_conditions_1
3D HN(CA)COsample_1isotropicsample_conditions_1
3D HNCACBsample_1isotropicsample_conditions_1
3D CBCA(CO)NHsample_1isotropicsample_conditions_1
3D HBHA(CO)NHsample_1isotropicsample_conditions_1
3D HBHANHsample_1isotropicsample_conditions_1
3D CCH-TOCSYsample_1isotropicsample_conditions_1
3D 1H-15N NOESYsample_1isotropicsample_conditions_1
3D 1H-13C NOESY aliphaticsample_1isotropicsample_conditions_1
3D 1H-13C NOESY aromaticsample_1isotropicsample_conditions_1

Software:

NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing

NMRView, Johnson, One Moon Scientific - chemical shift assignment

NMR spectrometers:

  • Bruker Avance 600 MHz

Download HSQC peak lists in one of the following formats:
CSV: Backbone or all simulated peaks
SPARKY: Backbone or all simulated peaks