BMRB Entry 25982

Title:
Peptide model of 4-stranded beta-arch.
Deposition date:
2016-03-05
Original release date:
2017-03-02
Authors:
Kung, Vanessa
Citation:

Citation: Kung, Vanessa. "A designed peptide model of early-stage amyloid structures"  .

Assembly members:

Assembly members:
entity, polymer, 31 residues, 3218.846 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity: XTEIRVXGVTIRMRXSHXFW VQVXXKEFKHX

Data sets:
Data typeCount
1H chemical shifts215

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1entity1

Entities:

Entity 1, entity 31 residues - 3218.846 Da.

1   NH2THRGLUILEARGVAL4FUGLYVALTHR
2   ILEARGMETARGDALSERHISDALPHETRP
3   VALGLNVALDPR4G6LYSGLUPHELYSHIS
4   ACE

Samples:

sample_1: entity 2 mM

sample_conditions_1: pH: 3.8; pressure: 1 atm; temperature: 273 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H COSYsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

X-PLOR_NIH v2.35, Schwieters, Kuszewski, Tjandra and Clore - structure solution

NMR spectrometers:

  • Bruker Avance 600 MHz