BMRB Entry 4975

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4975

NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry

Title:
Assignment of selectively 13C-labeled cellopentaose synthesized using an engineered glycosynthase
Deposition date:
2001-03-20
Original release date:
2001-10-08
Authors:
Brun, Emmanuel; Brummer, Harry; Mackenzie, Lloyd; Withers, Stephen; McIntosh, Lawrence
Citation:

Citation: Brun, Emmanuel; Brumer, Harry; Mackenzie, Lloyd; Withers, Stephen; McIntosh, Lawrence. "Letter to the Editor: Assignment of selectively 13C-labeled cellopentaose synthesized using an engineered glycosynthase"  J. Biomol. NMR 21, 67-68 (2001).

Assembly members:

Assembly members:
cellopentaose, polymer, 5 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: enzymatic semisynthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
cellopentaose: XXXXX

Data sets:
Data typeCount
13C chemical shifts6
1H chemical shifts7
coupling constants8

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1cellopentaose1

Entities:

Entity 1, cellopentaose 5 residues - Formula weight is not available

1   GLCGLCGLCGLCGLC

Samples:

sample_1: cellopentaose, [U-95% 13C]-Glc2, 3.3 mM

condition_1: pH: .; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
1H-13C HSQCsample_1not availablecondition_1
1H-13C HCCH-COSYsample_1not availablecondition_1

Software:

FELIX v2.3 - processing

NMR spectrometers:

  • Varian Unity 500 MHz