BMRB Entry 6412
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6412
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Citation: Sforca, Mauricio; Machado, Alessandra; Figueredo, Rita; Oyama, Sergio; Silva, Fernanda; Miranda, Antonio; Daffre, Sirlei; Miranda, M.; Spisni, Alberto; Pertinhez, Thelma. "The micelle-bound structure of an antimicrobial peptide derived from the
alpha-chain of bovine hemoglobin isolated from the tick Boophilus microplus." Biochemistry 44, 6440-6451 (2005).
PubMed: 15850378
Assembly members:
48-61 fragment, polymer, 14 residues, 1374.5 Da.
Natural source: Common Name: Cow Taxonomy ID: 9913 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Bos taurus
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
48-61 fragment: LSHGSAQVKGHGAK
- assigned_chemical_shifts
- coupling_constants
| Data type | Count |
| 1H chemical shifts | 83 |
| coupling constants | 13 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | 48-61 fragment | 1 |
Entities:
Entity 1, 48-61 fragment 14 residues - 1374.5 Da.
| 1 | LEU | SER | HIS | GLY | SER | ALA | GLN | VAL | LYS | GLY | ||||
| 2 | HIS | GLY | ALA | LYS |
Samples:
sample_1: 48-61 fragment 1.0 mM; sodium dodecyl sulfate (SDS) 200 mM
Ex-cond_1: pH: 4.0; temperature: 310 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H DQF-COSY | not available | not available | not available |
| NOESY | not available | not available | not available |
| ROESY | not available | not available | not available |
| TOCSY | not available | not available | not available |
Software:
NMRPIPE v5.0 -
NMRView v5.0 -
NMR spectrometers:
- Varian Inova 500 MHz