BMRB Entry 21082

Title:
HAL-2/27
Deposition date:
2018-09-19
Original release date:
2020-05-12
Authors:
Socha, Ondrej
Citation:

Citation: Kocendova, Jitka; Vankova, Eva; Volejnikova, Andrea; Nesuta, Ondrej; Hajek, Miroslav; Hadravova, Romana; Humpolickova, Jana; Budesinsky, Milos; Socha, Ondrej; Cerovsky, Vaclav. "HAL-2/27"  .

Assembly members:

Assembly members:
HAL-2/27, polymer, 13 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
HAL-2/27: GKWMKLLKKILKX

Data sets:
Data typeCount
13C chemical shifts72
15N chemical shifts12
1H chemical shifts117

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1polypeptide1

Entities:

Entity 1, polypeptide 13 residues - Formula weight is not available

1   GLYLYSTRPMETLYSLEULEULYSLYSILE
2   LEULYSNH2

Samples:

sample_1: TFE 30 v/v; H2O 95%; D2O, [U-2H], 5%

sample_conditions_1: pH: 4.4; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H COSYsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1
2D 1H-15N HSQCsample_1isotropicsample_conditions_1
2D 1H-13C HSQCsample_1isotropicsample_conditions_1

Software:

CcpNmr_Analysis v2.4, CCPN - chemical shift assignment, peak picking

X-PLOR_NIH v2.44, Schwieters, Kuszewski, Tjandra and Clore - refinement, structure solution

TOPSPIN, Bruker Biospin - collection, processing

TALOS, Cornilescu, Delaglio and Bax - data analysis

NMR spectrometers:

  • Bruker Avance 600 MHz

Download HSQC peak lists in one of the following formats:
CSV: Backbone or all simulated peaks
SPARKY: Backbone or all simulated peaks