BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
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BMRB Entry 4656

Title: Design and Solution Structure of a Well-folded Stack of Two Beta-hairpins Based on the Amino-terminal Fragment of Human Granulin A   PubMed: 10956026

Authors: Tolkatchev, D.; Ng, A.; Vranken, W.; Ni, F.

Citation: Tolkatchev, D.; Ng, A.; Vranken, W.; Ni, F.. "Design and Solution Structure of a Well-folded Stack of Two Beta-hairpins Based on the Amino-terminal Fragment of Human Granulin A"  Biochemistry 39, 2878-2886 (2000).

Assembly members:
GRANULIN_A, polymer, 31 residues, Formula weight is not available

Natural source:   Common Name: human   Taxonomy ID: 9606   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Homo sapiens

Experimental source:   Production method: .

Entity Sequences (FASTA):
GRANULIN_A: VVHCDMEVICPDGYTCCRLP SGAWGCCPFTQ

Data sets:
Data typeCount
1H chemical shifts192

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1GRANULIN A1

Entities:

Entity 1, GRANULIN A 31 residues - Formula weight is not available

1   VALVALHISCYSASPMETGLUVALILECYS
2   PROASPGLYTYRTHRCYSCYSARGLEUPRO
3   SERGLYALATRPGLYCYSCYSPROPHETHR
4   GLN

Samples:

sample_1: GRANULIN_A 0.5 mM; sodium acetate, [U-2H], 20 mM; D2O 10%; H2O 90%

sample_2: GRANULIN_A 0.5 mM; sodium acetate, [U-2H], 20 mM; D2O 100%

sample_cond_1: pH: 5.0; pressure: 1 atm; temperature: 288 K

sample_cond_2: pH: 5.0; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D NOESYnot availablenot availablenot available

Software:

X-PLOR v3.1 - refinement, structure solution

NMR spectrometers:

  • Bruker DRX 500 MHz

Related Database Links:

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