data_16669 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; GTPase RhoA GTPgS ; _BMRB_accession_number 16669 _BMRB_flat_file_name bmr16669.str _Entry_type original _Submission_date 2010-01-07 _Accession_date 2010-01-07 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details 'RhoA-GTPgS chemical shifts assignments' loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Gasmi-Seabrook Genevieve . . 2 Ikura Mitsu . . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count assigned_chemical_shifts 1 spectral_peak_list 1 stop_ loop_ _Data_type _Data_type_count "1H chemical shifts" 118 "13C chemical shifts" 313 "15N chemical shifts" 117 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2010-03-01 update BMRB 'completed entry citation' 2010-02-16 original author 'original release' stop_ loop_ _Related_BMRB_accession_number _Relationship 16668 RhoA-GDP stop_ save_ ############################# # Citation for this entry # ############################# save_RhoA-GTPgS _Saveframe_category entry_citation _Citation_full . _Citation_title 'Real-time NMR study of guanine nucleotide exchange and activation of RhoA by PDZ-RhoGEF.' _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 20018869 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Gasmi-Seabrook Genevieve M.C. . 2 Marshall Christopher B. . 3 Cheung Melissa . . 4 Kim Bryan . . 5 Wang Feng . . 6 Jang 'Ying Ju' . . 7 Mak Tak W. . 8 Stambolic Vuk . . 9 Ikura Mitsuhiko . . stop_ _Journal_abbreviation 'J. Biol. Chem.' _Journal_name_full 'The Journal of biological chemistry' _Journal_volume 285 _Journal_issue 8 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 5137 _Page_last 5145 _Year 2010 _Details . loop_ _Keyword GTPases NMR RhoA stop_ save_ ################################## # Molecular system description # ################################## save_assembly _Saveframe_category molecular_system _Mol_system_name 'RhoA GTPgS monomer' _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label protein $GTPase_RhoA nucleotide $GTPgS stop_ _System_molecular_weight 20.400 _System_physical_state native _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . loop_ _Biological_function GTPase stop_ _Database_query_date . _Details 'RhoA GTPgS bound form' save_ ######################## # Monomeric polymers # ######################## save_GTPase_RhoA _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common GTPase_RhoA _Molecular_mass 20.400 _Mol_thiol_state 'all free' loop_ _Biological_function GTPase stop_ _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 181 _Mol_residue_sequence ; MAAIRKKLVIVGDGACGKTC LLIVFSKDQFPEVYVPTVFE NYVADIEVDGKQVELALWDT AGQEDYDRLRPLSYPDTDVI LMCFSIDSPDSLENIPEKWT PEVKHFCPNVPIILVGNKKD LRNDEHTRRELAKMKQEPVK PEEGRDMANRIGAFGYMECS AKTKDGVREVFEMATRAALQ A ; loop_ _Residue_seq_code _Residue_label 1 MET 2 ALA 3 ALA 4 ILE 5 ARG 6 LYS 7 LYS 8 LEU 9 VAL 10 ILE 11 VAL 12 GLY 13 ASP 14 GLY 15 ALA 16 CYS 17 GLY 18 LYS 19 THR 20 CYS 21 LEU 22 LEU 23 ILE 24 VAL 25 PHE 26 SER 27 LYS 28 ASP 29 GLN 30 PHE 31 PRO 32 GLU 33 VAL 34 TYR 35 VAL 36 PRO 37 THR 38 VAL 39 PHE 40 GLU 41 ASN 42 TYR 43 VAL 44 ALA 45 ASP 46 ILE 47 GLU 48 VAL 49 ASP 50 GLY 51 LYS 52 GLN 53 VAL 54 GLU 55 LEU 56 ALA 57 LEU 58 TRP 59 ASP 60 THR 61 ALA 62 GLY 63 GLN 64 GLU 65 ASP 66 TYR 67 ASP 68 ARG 69 LEU 70 ARG 71 PRO 72 LEU 73 SER 74 TYR 75 PRO 76 ASP 77 THR 78 ASP 79 VAL 80 ILE 81 LEU 82 MET 83 CYS 84 PHE 85 SER 86 ILE 87 ASP 88 SER 89 PRO 90 ASP 91 SER 92 LEU 93 GLU 94 ASN 95 ILE 96 PRO 97 GLU 98 LYS 99 TRP 100 THR 101 PRO 102 GLU 103 VAL 104 LYS 105 HIS 106 PHE 107 CYS 108 PRO 109 ASN 110 VAL 111 PRO 112 ILE 113 ILE 114 LEU 115 VAL 116 GLY 117 ASN 118 LYS 119 LYS 120 ASP 121 LEU 122 ARG 123 ASN 124 ASP 125 GLU 126 HIS 127 THR 128 ARG 129 ARG 130 GLU 131 LEU 132 ALA 133 LYS 134 MET 135 LYS 136 GLN 137 GLU 138 PRO 139 VAL 140 LYS 141 PRO 142 GLU 143 GLU 144 GLY 145 ARG 146 ASP 147 MET 148 ALA 149 ASN 150 ARG 151 ILE 152 GLY 153 ALA 154 PHE 155 GLY 156 TYR 157 MET 158 GLU 159 CYS 160 SER 161 ALA 162 LYS 163 THR 164 LYS 165 ASP 166 GLY 167 VAL 168 ARG 169 GLU 170 VAL 171 PHE 172 GLU 173 MET 174 ALA 175 THR 176 ARG 177 ALA 178 ALA 179 LEU 180 GLN 181 ALA stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date 2015-07-29 loop_ _Database_name _Database_accession_code _Database_entry_mol_name _Sequence_query_to_submitted_percentage _Sequence_subject_length _Sequence_identity _Sequence_positive _Sequence_homology_expectation_value BMRB 16668 GTPase_RhoA 100.00 181 100.00 100.00 2.02e-130 PDB 1A2B "Human Rhoa Complexed With Gtp Analogue" 100.00 182 99.45 99.45 2.76e-129 PDB 1CC0 "Crystal Structure Of The Rhoa.Gdp-Rhogdi Complex" 100.00 190 99.45 99.45 6.72e-129 PDB 1CXZ "Crystal Structure Of Human Rhoa Complexed With The Effector Domain Of The Protein Kinase PknPRK1" 100.00 182 99.45 99.45 2.76e-129 PDB 1DPF "Crystal Structure Of A Mg-Free Form Of Rhoa Complexed With Gdp" 99.45 180 97.22 97.22 3.88e-125 PDB 1FTN "Crystal Structure Of The Human RhoaGDP COMPLEX" 100.00 193 99.45 99.45 4.42e-129 PDB 1KMQ "Crystal Structure Of A Constitutively Activated Rhoa Mutant (Q63l)" 99.45 184 97.78 98.33 1.30e-125 PDB 1LB1 "Crystal Structure Of The Dbl And Pleckstrin Homology Domains Of Dbs In Complex With Rhoa" 100.00 192 100.00 100.00 1.42e-130 PDB 1OW3 "Crystal Structure Of Rhoa.gdp.mgf3-in Complex With Rhogap" 100.00 193 99.45 99.45 4.42e-129 PDB 1S1C "Crystal Structure Of The Complex Between The Human Rhoa And Rho-Binding Domain Of Human Rocki" 100.00 183 100.00 100.00 1.61e-130 PDB 1TX4 "RhoRHOGAPGDP(DOT)ALF4 COMPLEX" 97.79 177 99.44 99.44 5.88e-126 PDB 1X86 "Crystal Structure Of The DhPH DOMAINS OF LEUKEMIA-Associated Rhogef In Complex With Rhoa" 100.00 196 100.00 100.00 3.48e-130 PDB 1XCG "Crystal Structure Of Human Rhoa In Complex With DhPH Fragment Of Pdzrhogef" 98.34 178 99.44 99.44 7.63e-127 PDB 2RGN "Crystal Structure Of P63rhogef Complex With Galpha-Q And Rhoa" 100.00 196 100.00 100.00 3.48e-130 PDB 3KZ1 "Crystal Structure Of The Complex Of Pdz-Rhogef DhPH DOMAINS WITH GTP- Gamma-S Activated Rhoa" 100.00 182 100.00 100.00 2.60e-130 PDB 3LW8 "Shigella Ipgb2 In Complex With Human Rhoa, Gdp And Mg2+ (Complex A)" 99.45 185 100.00 100.00 2.21e-129 PDB 3LWN "Shigella Ipgb2 In Complex With Human Rhoa, Gdp And Mg2+ (Complex B)" 99.45 185 100.00 100.00 2.21e-129 PDB 3LXR "Shigella Ipgb2 In Complex With Human Rhoa And Gdp (Complex C)" 99.45 185 100.00 100.00 2.21e-129 PDB 3MSX "Crystal Structure Of Rhoa.Gdp.Mgf3 In Complex With Gap Domain Of Arhgap20" 99.45 180 99.44 99.44 2.53e-128 PDB 3T06 "Crystal Structure Of The DhPH FRAGMENT OF PDZRHOGEF WITH N-Terminal Regulatory Elements In Complex With Human Rhoa" 98.34 178 99.44 99.44 7.63e-127 PDB 3TVD "Crystal Structure Of Mouse Rhoa-gtp Complex" 100.00 193 100.00 100.00 2.52e-130 PDB 4D0N "Akap13 (akap-lbc) Rhogef Domain In Complex With Rhoa" 100.00 185 100.00 100.00 1.90e-130 PDB 4F38 "Crystal Structure Of Geranylgeranylated Rhoa In Complex With Rhogdi In Its Active Gppnhp-Bound Form" 100.00 195 100.00 100.00 2.67e-130 PDB 4XH9 "Crystal Structure Of Human Rhoa In Complex With Dh/ph Fragment Of The Guanine Nucleotide Exchange Factor Net1" 98.90 180 99.44 99.44 2.28e-127 PDB 4XOI "Structure Of Hsanillin Bound With Rhoa(q63l) At 2.1 Angstroms Resolution" 99.45 180 98.89 98.89 3.52e-127 PDB 4XSG "The Complex Structure Of C3cer Exoenzyme And Gtp Bound Rhoa (nadh-free State)" 98.90 179 99.44 99.44 2.04e-127 PDB 4XSH "The Complex Structure Of C3cer Exoenzyme And Gtp Bound Rhoa (nadh- Bound State)" 98.90 179 99.44 99.44 2.04e-127 PDB 5A0F "Crystal Structure Of Yersinia Afp18-modified Rhoa" 100.00 181 100.00 100.00 2.02e-130 PDB 5BWM "The Complex Structure Of C3cer Exoenzyme And Gdp Bound Rhoa (nadh- Bound State)" 98.90 179 99.44 99.44 2.04e-127 DBJ BAA20863 "RhoA [Rattus norvegicus]" 94.48 174 100.00 100.00 4.04e-123 DBJ BAC36896 "unnamed protein product [Mus musculus]" 100.00 193 100.00 100.00 2.52e-130 DBJ BAC38971 "unnamed protein product [Mus musculus]" 100.00 193 100.00 100.00 2.52e-130 DBJ BAC99017 "Raichu-1237X [synthetic construct]" 100.00 777 100.00 100.00 1.49e-124 DBJ BAD96276 "ras homolog gene family, member A variant [Homo sapiens]" 100.00 193 99.45 99.45 9.77e-130 EMBL CAA28690 "unnamed protein product [Homo sapiens]" 100.00 193 100.00 100.00 2.26e-130 EMBL CAA39802 "rho1 [Canis lupus familiaris]" 100.00 193 99.45 99.45 1.53e-129 EMBL CAC08447 "RhoA GTPase [Gallus gallus]" 100.00 193 100.00 100.00 2.44e-130 EMBL CAC28868 "rho GTPase, partial [Platichthys flesus]" 70.17 127 98.43 100.00 8.52e-87 EMBL CAE46190 "hypothetical protein [Homo sapiens]" 100.00 193 100.00 100.00 2.26e-130 GB AAA30409 "rho (Gb) protein [Bos taurus]" 100.00 193 100.00 100.00 2.26e-130 GB AAA50612 "multidrug resistance protein, partial [Homo sapiens]" 97.79 189 100.00 100.00 3.08e-127 GB AAC18962 "GTPase cRhoA [Gallus gallus]" 100.00 193 100.00 100.00 2.44e-130 GB AAC23710 "Rho family GTPase [Mus musculus]" 100.00 193 99.45 99.45 9.50e-129 GB AAC33178 "GTP-binding protein [Homo sapiens]" 100.00 193 100.00 100.00 2.26e-130 REF NP_001003273 "transforming protein RhoA precursor [Canis lupus familiaris]" 100.00 193 100.00 100.00 2.26e-130 REF NP_001025020 "rho-related GTP-binding protein RhoC precursor [Gallus gallus]" 99.45 193 97.22 98.89 1.91e-126 REF NP_001038815 "transforming protein RhoA [Danio rerio]" 100.00 193 97.79 98.34 6.60e-127 REF NP_001079729 "ras homolog family member A [Xenopus laevis]" 100.00 193 97.79 98.90 4.79e-128 REF NP_001080441 "ras homolog family member A [Xenopus laevis]" 100.00 193 97.24 98.34 4.13e-127 SP P24406 "RecName: Full=Transforming protein RhoA; AltName: Full=Rho1; Flags: Precursor" 100.00 193 99.45 99.45 1.53e-129 SP P61585 "RecName: Full=Transforming protein RhoA; AltName: Full=Gb; AltName: Full=p21; Flags: Precursor" 100.00 193 100.00 100.00 2.26e-130 SP P61586 "RecName: Full=Transforming protein RhoA; AltName: Full=Rho cDNA clone 12; Short=h12; Flags: Precursor" 100.00 193 100.00 100.00 2.26e-130 SP P61589 "RecName: Full=Transforming protein RhoA; Flags: Precursor" 100.00 193 100.00 100.00 2.52e-130 SP Q5REY6 "RecName: Full=Transforming protein RhoA; Flags: Precursor" 100.00 193 100.00 100.00 2.26e-130 TPG DAA16889 "TPA: transforming protein RhoA precursor [Bos taurus]" 100.00 193 100.00 100.00 2.26e-130 stop_ save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $GTPase_RhoA Human 9606 Eukaryota Metazoa Homo sapiens stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name $GTPase_RhoA 'purified from the natural source' . Escherichia coli . pET28A stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type solution _Details . loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $GTPase_RhoA 0.3 mM '[U-100% 13C; U-100% 15N]' D2O 10 % 'natural abundance' H2O 90 % 'natural abundance' stop_ save_ ############################ # Computer software used # ############################ save_NMRView _Saveframe_category software _Name NMRView _Version . loop_ _Vendor _Address _Electronic_address 'Johnson, One Moon Scientific' . . stop_ loop_ _Task 'chemical shift assignment' stop_ _Details . save_ save_NMRPipe _Saveframe_category software _Name NMRPipe _Version . loop_ _Vendor _Address _Electronic_address 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . stop_ loop_ _Task 'data analysis' stop_ _Details . save_ save_NMRDraw _Saveframe_category software _Name NMRDraw _Version . loop_ _Vendor _Address _Electronic_address 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . stop_ loop_ _Task 'data analysis' stop_ _Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Varian _Model INOVA _Field_strength 600 _Details . save_ save_spectrometer_2 _Saveframe_category NMR_spectrometer _Manufacturer Bruker _Model Avance _Field_strength 800 _Details . save_ ############################# # NMR applied experiments # ############################# save_2D_1H-15N_HSQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_1 save_ save_3D_CBCA(CO)NH_2 _Saveframe_category NMR_applied_experiment _Experiment_name '3D CBCA(CO)NH' _Sample_label $sample_1 save_ save_3D_HNCACB_3 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCACB' _Sample_label $sample_1 save_ save_3D_HNCO_4 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HNCO' _Sample_label $sample_1 save_ save_3D_HN(CA)CO_5 _Saveframe_category NMR_applied_experiment _Experiment_name '3D HN(CA)CO' _Sample_label $sample_1 save_ save_3D_1H-15N_NOESY_6 _Saveframe_category NMR_applied_experiment _Experiment_name '3D 1H-15N NOESY' _Sample_label $sample_1 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details . loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units 'ionic strength' 100 . mM pH 7.0 . pH pressure 1 . atm temperature 293 . K stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Saveframe_category chemical_shift_reference _Details . loop_ _Mol_common_name _Atom_type _Atom_isotope_number _Atom_group _Chem_shift_units _Chem_shift_value _Reference_method _Reference_type _External_reference_sample_geometry _External_reference_location _External_reference_axis _Indirect_shift_ratio DSS C 13 'methyl protons' ppm 0.00 na indirect . . . 0.251449530 DSS H 1 'methyl protons' ppm 0.00 internal direct . . . 1.000000000 DSS N 15 'methyl protons' ppm 0.00 na indirect . . . 0.101329118 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assignments_RhoA _Saveframe_category assigned_chemical_shifts _Details . loop_ _Experiment_label '2D 1H-15N HSQC' '3D CBCA(CO)NH' '3D HNCACB' '3D HNCO' '3D HN(CA)CO' '3D 1H-15N NOESY' stop_ loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Chem_shift_reference_set_label $chemical_shift_reference_1 _Mol_system_component_name protein _Text_data_format . _Text_data . loop_ _Atom_shift_assign_ID _Residue_author_seq_code _Residue_seq_code _Residue_label _Atom_name _Atom_type _Chem_shift_value _Chem_shift_value_error _Chem_shift_ambiguity_code 1 1 1 MET H H 8.330 . 1 2 1 1 MET C C 175.470 . 1 3 1 1 MET CA C 55.510 . 1 4 1 1 MET CB C 33.160 . 1 5 1 1 MET N N 122.240 . 1 6 2 2 ALA H H 8.420 . 1 7 2 2 ALA C C 177.090 . 1 8 2 2 ALA CA C 52.190 . 1 9 2 2 ALA CB C 19.280 . 1 10 2 2 ALA N N 125.440 . 1 11 3 3 ALA H H 8.240 . 1 12 3 3 ALA C C 177.420 . 1 13 3 3 ALA CA C 52.340 . 1 14 3 3 ALA CB C 19.700 . 1 15 3 3 ALA N N 123.590 . 1 16 4 4 ILE H H 8.200 . 1 17 4 4 ILE C C 174.350 . 1 18 4 4 ILE CA C 61.150 . 1 19 4 4 ILE CB C 39.650 . 1 20 4 4 ILE N N 121.910 . 1 21 5 5 ARG H H 8.560 . 1 22 5 5 ARG CA C 55.220 . 1 23 5 5 ARG CB C 31.820 . 1 24 5 5 ARG N N 127.830 . 1 25 6 6 LYS C C 173.700 . 1 26 6 6 LYS CA C 52.330 . 1 27 6 6 LYS CB C 36.690 . 1 28 7 7 LYS H H 10.610 . 1 29 7 7 LYS C C 173.840 . 1 30 7 7 LYS CA C 56.700 . 1 31 7 7 LYS N N 124.780 . 1 32 8 8 LEU H H 9.510 . 1 33 8 8 LEU C C 174.430 . 1 34 8 8 LEU CA C 53.600 . 1 35 8 8 LEU CB C 45.990 . 1 36 8 8 LEU N N 134.000 . 1 37 9 9 VAL H H 8.110 . 1 38 9 9 VAL CA C 60.860 . 1 39 9 9 VAL CB C 34.860 . 1 40 9 9 VAL N N 125.750 . 1 41 10 10 ILE H H 8.230 . 1 42 10 10 ILE N N 127.080 . 1 43 11 11 VAL H H 8.680 . 1 44 11 11 VAL N N 117.430 . 1 45 14 14 GLY H H 8.670 . 1 46 14 14 GLY N N 106.690 . 1 47 16 16 CYS H H 7.970 . 1 48 16 16 CYS C C 173.550 . 1 49 16 16 CYS N N 115.600 . 1 50 17 17 GLY H H 8.030 . 1 51 17 17 GLY N N 109.410 . 1 52 26 26 SER H H 8.130 . 1 53 26 26 SER N N 111.150 . 1 54 27 27 LYS H H 8.740 . 1 55 27 27 LYS N N 119.520 . 1 56 28 28 ASP H H 7.790 . 1 57 28 28 ASP C C 174.690 . 1 58 28 28 ASP CA C 55.440 . 1 59 28 28 ASP CB C 40.420 . 1 60 28 28 ASP N N 119.140 . 1 61 29 29 GLN H H 6.660 . 1 62 29 29 GLN CA C 54.000 . 1 63 29 29 GLN N N 114.000 . 1 64 46 46 ILE C C 171.160 . 1 65 47 47 GLU H H 8.100 . 1 66 47 47 GLU C C 175.980 . 1 67 47 47 GLU CA C 54.170 . 1 68 47 47 GLU CB C 31.400 . 1 69 47 47 GLU N N 127.080 . 1 70 48 48 VAL H H 8.590 . 1 71 48 48 VAL C C 174.460 . 1 72 48 48 VAL CA C 60.440 . 1 73 48 48 VAL CB C 35.630 . 1 74 48 48 VAL N N 123.880 . 1 75 49 49 ASP H H 9.270 . 1 76 49 49 ASP C C 175.980 . 1 77 49 49 ASP CA C 55.510 . 1 78 49 49 ASP CB C 39.010 . 1 79 49 49 ASP N N 125.480 . 1 80 50 50 GLY H H 8.790 . 1 81 50 50 GLY C C 174.070 . 1 82 50 50 GLY CA C 45.430 . 1 83 50 50 GLY N N 103.700 . 1 84 51 51 LYS H H 8.180 . 1 85 51 51 LYS C C 174.570 . 1 86 51 51 LYS CA C 54.660 . 1 87 51 51 LYS CB C 33.800 . 1 88 51 51 LYS N N 121.740 . 1 89 52 52 GLN H H 8.280 . 1 90 52 52 GLN C C 175.020 . 1 91 52 52 GLN CA C 55.510 . 1 92 52 52 GLN CB C 28.650 . 1 93 52 52 GLN N N 122.390 . 1 94 53 53 VAL H H 9.150 . 1 95 53 53 VAL CA C 60.650 . 1 96 53 53 VAL CB C 35.070 . 1 97 53 53 VAL N N 126.930 . 1 98 68 68 ARG C C 176.370 . 1 99 68 68 ARG CA C 58.890 . 1 100 68 68 ARG CB C 29.150 . 1 101 69 69 LEU H H 7.410 . 1 102 69 69 LEU CA C 60.930 . 1 103 69 69 LEU CB C 42.400 . 1 104 69 69 LEU N N 113.320 . 1 105 72 72 LEU H H 7.400 . 1 106 72 72 LEU C C 178.750 . 1 107 72 72 LEU N N 116.990 . 1 108 73 73 SER H H 8.090 . 1 109 73 73 SER C C 174.690 . 1 110 73 73 SER N N 112.050 . 1 111 74 74 TYR H H 6.720 . 1 112 74 74 TYR N N 119.680 . 1 113 75 75 PRO C C 175.610 . 1 114 75 75 PRO CA C 66.290 . 1 115 76 76 ASP H H 8.910 . 1 116 76 76 ASP CB C 39.150 . 1 117 76 76 ASP N N 117.410 . 1 118 77 77 THR H H 7.440 . 1 119 77 77 THR N N 116.530 . 1 120 78 78 ASP H H 8.950 . 1 121 78 78 ASP N N 122.500 . 1 122 79 79 VAL H H 7.840 . 1 123 79 79 VAL N N 116.600 . 1 124 80 80 ILE C C 175.650 . 1 125 80 80 ILE CA C 57.410 . 1 126 80 80 ILE CB C 40.780 . 1 127 81 81 LEU H H 8.820 . 1 128 81 81 LEU N N 126.140 . 1 129 84 84 PHE C C 172.140 . 1 130 84 84 PHE CA C 56.140 . 1 131 84 84 PHE CB C 39.860 . 1 132 85 85 SER H H 9.370 . 1 133 85 85 SER N N 113.480 . 1 134 86 86 ILE C C 175.050 . 1 135 86 86 ILE CA C 64.530 . 1 136 87 87 ASP H H 8.150 . 1 137 87 87 ASP C C 174.070 . 1 138 87 87 ASP CA C 53.180 . 1 139 87 87 ASP CB C 41.830 . 1 140 87 87 ASP N N 115.280 . 1 141 88 88 SER H H 7.920 . 1 142 88 88 SER CA C 53.390 . 1 143 88 88 SER CB C 62.980 . 1 144 88 88 SER N N 110.130 . 1 145 89 89 PRO C C 178.870 . 1 146 89 89 PRO CA C 65.730 . 1 147 89 89 PRO CB C 31.900 . 1 148 90 90 ASP H H 9.080 . 1 149 90 90 ASP C C 178.020 . 1 150 90 90 ASP CA C 57.690 . 1 151 90 90 ASP CB C 40.140 . 1 152 90 90 ASP N N 118.770 . 1 153 91 91 SER H H 8.360 . 1 154 91 91 SER C C 177.090 . 1 155 91 91 SER CA C 61.570 . 1 156 91 91 SER CB C 63.540 . 1 157 91 91 SER N N 117.450 . 1 158 92 92 LEU H H 7.160 . 1 159 92 92 LEU C C 179.040 . 1 160 92 92 LEU CA C 56.990 . 1 161 92 92 LEU CB C 40.560 . 1 162 92 92 LEU N N 124.560 . 1 163 93 93 GLU H H 7.830 . 1 164 93 93 GLU C C 178.440 . 1 165 93 93 GLU CA C 58.960 . 1 166 93 93 GLU CB C 28.650 . 1 167 93 93 GLU N N 119.810 . 1 168 94 94 ASN H H 7.570 . 1 169 94 94 ASN CA C 53.890 . 1 170 94 94 ASN CB C 38.880 . 1 171 94 94 ASN N N 113.200 . 1 172 95 95 ILE H H 8.420 . 1 173 95 95 ILE N N 123.670 . 1 174 96 96 PRO C C 176.910 . 1 175 96 96 PRO CA C 65.090 . 1 176 96 96 PRO CB C 31.050 . 1 177 97 97 GLU H H 6.530 . 1 178 97 97 GLU C C 175.610 . 1 179 97 97 GLU CA C 57.620 . 1 180 97 97 GLU CB C 31.190 . 1 181 97 97 GLU N N 115.660 . 1 182 98 98 LYS H H 7.900 . 1 183 98 98 LYS C C 177.700 . 1 184 98 98 LYS CA C 57.270 . 1 185 98 98 LYS CB C 34.930 . 1 186 98 98 LYS N N 116.570 . 1 187 99 99 TRP H H 7.530 . 1 188 99 99 TRP C C 177.480 . 1 189 99 99 TRP CA C 60.370 . 1 190 99 99 TRP CB C 29.920 . 1 191 99 99 TRP N N 120.590 . 1 192 100 100 THR H H 8.980 . 1 193 100 100 THR N N 114.780 . 1 194 101 101 PRO C C 178.050 . 1 195 101 101 PRO CA C 65.870 . 1 196 101 101 PRO CB C 31.050 . 1 197 102 102 GLU H H 6.980 . 1 198 102 102 GLU C C 178.050 . 1 199 102 102 GLU CA C 60.720 . 1 200 102 102 GLU CB C 30.130 . 1 201 102 102 GLU N N 116.690 . 1 202 103 103 VAL H H 8.560 . 1 203 103 103 VAL C C 178.130 . 1 204 103 103 VAL CA C 66.850 . 1 205 103 103 VAL CB C 31.610 . 1 206 103 103 VAL N N 116.450 . 1 207 104 104 LYS H H 8.720 . 1 208 104 104 LYS CA C 58.540 . 1 209 104 104 LYS N N 117.140 . 1 210 105 105 HIS H H 7.420 . 1 211 105 105 HIS N N 115.930 . 1 212 106 106 PHE H H 7.430 . 1 213 106 106 PHE C C 177.820 . 1 214 106 106 PHE CA C 55.580 . 1 215 106 106 PHE CB C 39.370 . 1 216 106 106 PHE N N 113.390 . 1 217 107 107 CYS H H 7.430 . 1 218 107 107 CYS CA C 58.750 . 1 219 107 107 CYS CB C 29.000 . 1 220 107 107 CYS N N 116.560 . 1 221 108 108 PRO C C 177.530 . 1 222 108 108 PRO CA C 64.950 . 1 223 108 108 PRO CB C 31.610 . 1 224 109 109 ASN H H 8.800 . 1 225 109 109 ASN C C 174.450 . 1 226 109 109 ASN CA C 53.900 . 1 227 109 109 ASN CB C 38.450 . 1 228 109 109 ASN N N 113.750 . 1 229 110 110 VAL H H 7.060 . 1 230 110 110 VAL CA C 60.230 . 1 231 110 110 VAL CB C 33.300 . 1 232 110 110 VAL N N 121.980 . 1 233 111 111 PRO CA C 63.120 . 1 234 111 111 PRO CB C 32.390 . 1 235 112 112 ILE H H 8.280 . 1 236 112 112 ILE C C 175.750 . 1 237 112 112 ILE CA C 54.850 . 1 238 112 112 ILE CB C 42.610 . 1 239 112 112 ILE N N 119.970 . 1 240 113 113 ILE H H 9.170 . 1 241 113 113 ILE C C 174.480 . 1 242 113 113 ILE CA C 59.450 . 1 243 113 113 ILE CB C 37.950 . 1 244 113 113 ILE N N 127.680 . 1 245 114 114 LEU H H 8.420 . 1 246 114 114 LEU C C 173.560 . 1 247 114 114 LEU CA C 53.880 . 1 248 114 114 LEU CB C 43.740 . 1 249 114 114 LEU N N 130.470 . 1 250 115 115 VAL H H 9.160 . 1 251 115 115 VAL C C 174.200 . 1 252 115 115 VAL CA C 60.580 . 1 253 115 115 VAL N N 128.400 . 1 254 116 116 GLY H H 8.460 . 1 255 116 116 GLY CA C 45.150 . 1 256 116 116 GLY N N 111.960 . 1 257 118 118 LYS C C 178.730 . 1 258 118 118 LYS CB C 29.080 . 1 259 119 119 LYS H H 8.780 . 1 260 119 119 LYS C C 177.400 . 1 261 119 119 LYS CA C 59.170 . 1 262 119 119 LYS CB C 32.390 . 1 263 119 119 LYS N N 116.240 . 1 264 120 120 ASP H H 8.820 . 1 265 120 120 ASP C C 176.380 . 1 266 120 120 ASP CA C 55.440 . 1 267 120 120 ASP CB C 40.350 . 1 268 120 120 ASP N N 115.510 . 1 269 121 121 LEU H H 8.160 . 1 270 121 121 LEU C C 177.820 . 1 271 121 121 LEU CA C 55.150 . 1 272 121 121 LEU CB C 40.710 . 1 273 121 121 LEU N N 118.340 . 1 274 122 122 ARG H H 7.380 . 1 275 122 122 ARG C C 175.640 . 1 276 122 122 ARG CA C 60.300 . 1 277 122 122 ARG CB C 29.570 . 1 278 122 122 ARG N N 118.020 . 1 279 123 123 ASN H H 7.770 . 1 280 123 123 ASN C C 174.410 . 1 281 123 123 ASN CA C 51.560 . 1 282 123 123 ASN CB C 38.730 . 1 283 123 123 ASN N N 111.730 . 1 284 124 124 ASP H H 7.100 . 1 285 124 124 ASP C C 175.730 . 1 286 124 124 ASP CA C 54.100 . 1 287 124 124 ASP CB C 44.160 . 1 288 124 124 ASP N N 121.300 . 1 289 125 125 GLU H H 9.210 . 1 290 125 125 GLU C C 178.280 . 1 291 125 125 GLU CA C 59.950 . 1 292 125 125 GLU CB C 30.200 . 1 293 125 125 GLU N N 130.000 . 1 294 126 126 HIS H H 8.510 . 1 295 126 126 HIS C C 177.010 . 1 296 126 126 HIS CA C 60.230 . 1 297 126 126 HIS CB C 29.570 . 1 298 126 126 HIS N N 119.780 . 1 299 127 127 THR H H 8.340 . 1 300 127 127 THR C C 176.320 . 1 301 127 127 THR CA C 67.210 . 1 302 127 127 THR CB C 69.110 . 1 303 127 127 THR N N 117.870 . 1 304 128 128 ARG H H 8.280 . 1 305 128 128 ARG C C 179.620 . 1 306 128 128 ARG CA C 60.720 . 1 307 128 128 ARG CB C 30.200 . 1 308 128 128 ARG N N 118.760 . 1 309 129 129 ARG H H 8.380 . 1 310 129 129 ARG C C 179.350 . 1 311 129 129 ARG CA C 59.520 . 1 312 129 129 ARG CB C 30.550 . 1 313 129 129 ARG N N 120.900 . 1 314 130 130 GLU H H 8.400 . 1 315 130 130 GLU C C 180.670 . 1 316 130 130 GLU CA C 59.520 . 1 317 130 130 GLU CB C 30.620 . 1 318 130 130 GLU N N 120.070 . 1 319 131 131 LEU H H 8.470 . 1 320 131 131 LEU C C 180.390 . 1 321 131 131 LEU CA C 57.760 . 1 322 131 131 LEU CB C 41.620 . 1 323 131 131 LEU N N 119.520 . 1 324 132 132 ALA H H 8.110 . 1 325 132 132 ALA HA H 17.870 . 1 326 132 132 ALA C C 181.740 . 1 327 132 132 ALA CA C 55.220 . 1 328 132 132 ALA N N 122.260 . 1 329 133 133 LYS H H 7.480 . 1 330 133 133 LYS C C 177.860 . 1 331 133 133 LYS CA C 59.450 . 1 332 133 133 LYS CB C 32.670 . 1 333 133 133 LYS N N 119.590 . 1 334 134 134 MET H H 7.410 . 1 335 134 134 MET C C 177.860 . 1 336 134 134 MET CA C 53.530 . 1 337 134 134 MET CB C 31.960 . 1 338 134 134 MET N N 115.980 . 1 339 135 135 LYS H H 8.000 . 1 340 135 135 LYS C C 175.360 . 1 341 135 135 LYS CA C 57.410 . 1 342 135 135 LYS CB C 28.870 . 1 343 135 135 LYS N N 114.740 . 1 344 136 136 GLN H H 7.890 . 1 345 136 136 GLN C C 175.190 . 1 346 136 136 GLN CA C 53.880 . 1 347 136 136 GLN CB C 34.080 . 1 348 136 136 GLN N N 116.110 . 1 349 137 137 GLU H H 8.280 . 1 350 137 137 GLU CA C 54.170 . 1 351 137 137 GLU CB C 31.680 . 1 352 137 137 GLU N N 119.340 . 1 353 138 138 PRO C C 175.960 . 1 354 138 138 PRO CA C 63.190 . 1 355 138 138 PRO CB C 32.320 . 1 356 139 139 VAL H H 8.830 . 1 357 139 139 VAL C C 176.780 . 1 358 139 139 VAL CA C 64.320 . 1 359 139 139 VAL N N 123.520 . 1 360 140 140 LYS H H 9.190 . 1 361 140 140 LYS CA C 54.660 . 1 362 140 140 LYS CB C 32.460 . 1 363 140 140 LYS N N 130.510 . 1 364 141 141 PRO C C 179.290 . 1 365 141 141 PRO CA C 66.010 . 1 366 141 141 PRO CB C 31.610 . 1 367 142 142 GLU H H 9.570 . 1 368 142 142 GLU C C 178.750 . 1 369 142 142 GLU CA C 59.740 . 1 370 142 142 GLU CB C 28.650 . 1 371 142 142 GLU N N 115.180 . 1 372 143 143 GLU H H 7.250 . 1 373 143 143 GLU C C 180.560 . 1 374 143 143 GLU CA C 58.540 . 1 375 143 143 GLU CB C 29.780 . 1 376 143 143 GLU N N 118.900 . 1 377 144 144 GLY H H 7.410 . 1 378 144 144 GLY C C 174.320 . 1 379 144 144 GLY CA C 46.630 . 1 380 144 144 GLY N N 108.370 . 1 381 145 145 ARG H H 7.660 . 1 382 145 145 ARG C C 178.860 . 1 383 145 145 ARG CA C 59.380 . 1 384 145 145 ARG CB C 29.920 . 1 385 145 145 ARG N N 121.200 . 1 386 146 146 ASP H H 7.950 . 1 387 146 146 ASP C C 179.040 . 1 388 146 146 ASP CA C 57.200 . 1 389 146 146 ASP CB C 40.570 . 1 390 146 146 ASP N N 118.800 . 1 391 147 147 MET H H 7.590 . 1 392 147 147 MET C C 177.460 . 1 393 147 147 MET CA C 56.770 . 1 394 147 147 MET CB C 29.640 . 1 395 147 147 MET N N 120.470 . 1 396 148 148 ALA H H 8.210 . 1 397 148 148 ALA C C 179.090 . 1 398 148 148 ALA CA C 55.080 . 1 399 148 148 ALA CB C 18.570 . 1 400 148 148 ALA N N 121.730 . 1 401 149 149 ASN H H 7.780 . 1 402 149 149 ASN C C 178.190 . 1 403 149 149 ASN CA C 55.720 . 1 404 149 149 ASN CB C 38.170 . 1 405 149 149 ASN N N 115.970 . 1 406 150 150 ARG H H 8.210 . 1 407 150 150 ARG C C 178.950 . 1 408 150 150 ARG CA C 59.740 . 1 409 150 150 ARG CB C 30.480 . 1 410 150 150 ARG N N 122.470 . 1 411 151 151 ILE H H 7.890 . 1 412 151 151 ILE C C 176.200 . 1 413 151 151 ILE CA C 61.640 . 1 414 151 151 ILE CB C 38.730 . 1 415 151 151 ILE N N 108.960 . 1 416 152 152 GLY H H 7.630 . 1 417 152 152 GLY C C 175.920 . 1 418 152 152 GLY CA C 46.340 . 1 419 152 152 GLY N N 110.610 . 1 420 153 153 ALA H H 8.560 . 1 421 153 153 ALA C C 176.750 . 1 422 153 153 ALA CA C 52.620 . 1 423 153 153 ALA CB C 19.140 . 1 424 153 153 ALA N N 122.100 . 1 425 154 154 PHE H H 9.770 . 1 426 154 154 PHE C C 175.960 . 1 427 154 154 PHE CA C 60.160 . 1 428 154 154 PHE CB C 40.070 . 1 429 154 154 PHE N N 125.030 . 1 430 155 155 GLY H H 7.300 . 1 431 155 155 GLY C C 174.370 . 1 432 155 155 GLY CA C 45.080 . 1 433 155 155 GLY N N 99.910 . 1 434 156 156 TYR H H 8.280 . 1 435 156 156 TYR C C 174.150 . 1 436 156 156 TYR CA C 55.580 . 1 437 156 156 TYR CB C 42.190 . 1 438 156 156 TYR N N 119.940 . 1 439 157 157 MET H H 8.250 . 1 440 157 157 MET C C 172.520 . 1 441 157 157 MET CA C 52.470 . 1 442 157 157 MET CB C 37.250 . 1 443 157 157 MET N N 125.780 . 1 444 158 158 GLU H H 7.830 . 1 445 158 158 GLU C C 176.740 . 1 446 158 158 GLU CA C 53.390 . 1 447 158 158 GLU CB C 33.160 . 1 448 158 158 GLU N N 116.200 . 1 449 159 159 CYS H H 9.160 . 1 450 159 159 CYS C C 172.120 . 1 451 159 159 CYS CA C 55.930 . 1 452 159 159 CYS CB C 31.970 . 1 453 159 159 CYS N N 114.830 . 1 454 160 160 SER H H 8.830 . 1 455 160 160 SER CA C 56.000 . 1 456 160 160 SER CB C 64.950 . 1 457 160 160 SER N N 111.800 . 1 458 162 162 LYS C C 177.570 . 1 459 162 162 LYS CA C 58.750 . 1 460 162 162 LYS CB C 32.950 . 1 461 163 163 THR H H 7.910 . 1 462 163 163 THR C C 175.330 . 1 463 163 163 THR CA C 61.360 . 1 464 163 163 THR CB C 69.390 . 1 465 163 163 THR N N 106.100 . 1 466 164 164 LYS H H 7.870 . 1 467 164 164 LYS C C 175.390 . 1 468 164 164 LYS CA C 60.160 . 1 469 164 164 LYS CB C 30.270 . 1 470 164 164 LYS N N 118.050 . 1 471 165 165 ASP H H 7.920 . 1 472 165 165 ASP C C 177.340 . 1 473 165 165 ASP CA C 55.160 . 1 474 165 165 ASP CB C 42.190 . 1 475 165 165 ASP N N 122.070 . 1 476 166 166 GLY H H 9.170 . 1 477 166 166 GLY C C 174.600 . 1 478 166 166 GLY CA C 46.700 . 1 479 166 166 GLY N N 115.480 . 1 480 167 167 VAL H H 7.360 . 1 481 167 167 VAL C C 177.110 . 1 482 167 167 VAL CA C 67.350 . 1 483 167 167 VAL CB C 31.680 . 1 484 167 167 VAL N N 119.950 . 1 485 168 168 ARG H H 8.670 . 1 486 168 168 ARG C C 178.410 . 1 487 168 168 ARG CA C 60.230 . 1 488 168 168 ARG CB C 28.930 . 1 489 168 168 ARG N N 119.090 . 1 490 169 169 GLU H H 9.430 . 1 491 169 169 GLU C C 179.970 . 1 492 169 169 GLU CA C 61.500 . 1 493 169 169 GLU CB C 28.650 . 1 494 169 169 GLU N N 118.330 . 1 495 170 170 VAL H H 7.780 . 1 496 170 170 VAL C C 176.560 . 1 497 170 170 VAL CA C 67.140 . 1 498 170 170 VAL CB C 31.330 . 1 499 170 170 VAL N N 121.100 . 1 500 171 171 PHE H H 6.960 . 1 501 171 171 PHE C C 179.270 . 1 502 171 171 PHE CA C 62.840 . 1 503 171 171 PHE CB C 41.900 . 1 504 171 171 PHE N N 116.430 . 1 505 172 172 GLU H H 9.050 . 1 506 172 172 GLU CA C 60.370 . 1 507 172 172 GLU N N 124.650 . 1 508 173 173 MET C C 178.020 . 1 509 173 173 MET CA C 59.240 . 1 510 173 173 MET CB C 32.950 . 1 511 174 174 ALA H H 8.200 . 1 512 174 174 ALA C C 178.380 . 1 513 174 174 ALA CA C 54.730 . 1 514 174 174 ALA CB C 18.640 . 1 515 174 174 ALA N N 118.990 . 1 516 175 175 THR H H 7.910 . 1 517 175 175 THR C C 175.860 . 1 518 175 175 THR CA C 63.120 . 1 519 175 175 THR CB C 67.560 . 1 520 175 175 THR N N 114.280 . 1 521 176 176 ARG H H 8.200 . 1 522 176 176 ARG C C 179.520 . 1 523 176 176 ARG CA C 61.140 . 1 524 176 176 ARG N N 120.820 . 1 525 177 177 ALA H H 7.980 . 1 526 177 177 ALA C C 179.610 . 1 527 177 177 ALA CA C 55.160 . 1 528 177 177 ALA CB C 16.670 . 1 529 177 177 ALA N N 120.480 . 1 530 178 178 ALA H H 7.790 . 1 531 178 178 ALA C C 178.470 . 1 532 178 178 ALA CA C 53.880 . 1 533 178 178 ALA CB C 17.300 . 1 534 178 178 ALA N N 119.100 . 1 535 179 179 LEU H H 7.860 . 1 536 179 179 LEU C C 177.840 . 1 537 179 179 LEU CA C 55.650 . 1 538 179 179 LEU CB C 42.320 . 1 539 179 179 LEU N N 116.130 . 1 540 180 180 GLN H H 7.410 . 1 541 180 180 GLN C C 174.770 . 1 542 180 180 GLN CA C 56.700 . 1 543 180 180 GLN CB C 29.430 . 1 544 180 180 GLN N N 118.240 . 1 545 181 181 ALA H H 7.710 . 1 546 181 181 ALA CA C 54.310 . 1 547 181 181 ALA CB C 20.120 . 1 548 181 181 ALA N N 130.010 . 1 stop_ save_ save_spectral_peak_list_GTPgS_hsqc _Saveframe_category spectral_peak_list _Details . loop_ _Software_label $NMRView stop_ _Experiment_label '2D 1H-15N HSQC' _Number_of_spectral_dimensions 2 loop_ _Expt_dimension_ID _Atom_type _Spectral_region 2 H H 2 N N stop_ _Sample_label $sample_1 _Sample_conditions_label $sample_conditions_1 _Text_data_format "NMR-STAR v3" _Text_data ; >>save_spectral_peak_list_GTPgS_hsqc >> _Spectral_peak_list.Sf_category spectral_peak_list >> _Spectral_peak_list.Sf_framecode spectral_peak_list_GTPgS_hsqc >> _Spectral_peak_list.Entry_ID 16669 >> _Spectral_peak_list.ID 1 >> _Spectral_peak_list.Sample_ID 1 >> _Spectral_peak_list.Sample_label $sample_1 >> _Spectral_peak_list.Sample_condition_list_ID 1 >> _Spectral_peak_list.Sample_condition_list_label $sample_conditions_1 >> _Spectral_peak_list.Experiment_ID 1 >> _Spectral_peak_list.Experiment_name '2D 1H-15N HSQC' >> _Spectral_peak_list.Number_of_spectral_dimensions 2 >> _Spectral_peak_list.Details . >> _Spectral_peak_list.Text_data_format text >> _Spectral_peak_list.Text_data >>; >>loop_ >> _Peak_list_number >> _Intensity_height >> _Intensity_volume >> _Intensity_volume2 >> _Peak_status >> _flag >> _comment >> _Dim_1_label >> _Dim_1_chem_shift >> _Dim_1_line_width >> _Dim_1_bounds >> _Dim_1_error >> _Dim_1_j >> _Dim_1_link0 >> _Dim_1_link1 >> _Dim_1_thread >> _Dim_1_user >> _Dim_2_label >> _Dim_2_chem_shift >> _Dim_2_line_width >> _Dim_2_bounds >> _Dim_2_error >> _Dim_2_j >> _Dim_2_link0 >> _Dim_2_link1 >> _Dim_2_thread >> _Dim_2_user >> >> 0 0.033 0.000 0.000 0 2 {?} >>{?} 11.62913036 0.04479000 0.08143000 {++} 0.00000000 0 0 0 {?} >>{?} 132.69013977 0.24792001 0.47490001 {++} 0.00000000 0 0 0 {?} >> 1 0.034 0.000 0.000 0 2 {?} >>{?} 10.61452961 0.04193000 0.07567000 {++} 0.00000000 0 0 0 {?} >>{?} 124.77760315 0.31676999 0.58078003 {++} 0.00000000 0 0 0 {?} >> 2 0.013 0.000 0.000 0 2 {?} >>{?} 10.19151020 0.04074000 0.04069000 {++} 0.00000000 0 0 0 {?} >>{?} 117.36636353 0.48967001 0.48921999 {++} 0.00000000 0 0 0 {?} >> 3 0.036 0.000 0.000 0 2 {?} >>{?} 10.05430984 0.04785000 0.08592000 {+P} 0.00000000 0 0 0 {?} >>{?} 129.39167786 0.32661000 0.57086003 {++} 0.00000000 0 0 0 {?} >> 4 0.039 0.000 0.000 0 2 {?} >>{?} 9.77530956 0.04391000 0.08984000 {++} 0.00000000 0 0 0 {?} >>{?} 125.02604675 0.27366000 0.49101001 {++} 0.00000000 0 0 0 {?} >> 5 0.011 0.000 0.000 0 2 {?} >>{?} 9.64451027 0.04512000 0.04512000 {++} 0.00000000 0 0 0 {?} >>{?} 127.79904938 0.39658001 0.35275000 {++} 0.00000000 0 0 0 {?} >> 6 0.020 0.000 0.000 0 2 {?} >>{?} 9.59125042 0.04532000 0.08592000 {P+} 0.00000000 0 0 0 {?} >>{?} 134.27070618 0.21760000 0.29075000 {++} 0.00000000 0 0 0 {?} >> 7 0.012 0.000 0.000 0 2 {?} >>{?} 9.56398010 0.04341000 0.03928000 {++} 0.00000000 0 0 0 {?} >>{?} 118.88327789 0.35122001 0.32820001 {++} 0.00000000 0 0 0 {?} >> 8 0.087 0.000 0.000 0 2 {?} >>{?} 9.57161045 0.03123000 0.08479000 {++} 0.00000000 0 0 0 {?} >>{?} 115.15823364 0.24571000 0.55322999 {++} 0.00000000 0 0 0 {?} >> 9 0.031 0.000 0.000 0 2 {?} >>{?} 9.51144981 0.05490000 0.13999000 {++} 0.00000000 0 0 0 {?} >>{?} 133.99143982 0.32912999 0.56545001 {++} 0.00000000 0 0 0 {?} >> 10 0.087 0.000 0.000 0 2 {?} >>{?} 9.43041039 0.03978000 0.09519000 {++} 0.00000000 0 0 0 {?} >>{?} 118.32858276 0.31703001 0.57088000 {++} 0.00000000 0 0 0 {?} >> 11 0.030 0.000 0.000 0 2 {?} >>{?} 9.37528992 0.05543000 0.07751000 {++} 0.00000000 0 0 0 {?} >>{?} 113.48004913 0.29683000 0.49210000 {++} 0.00000000 0 0 0 {?} >> 12 0.026 0.000 0.000 0 2 {?} >>{?} 9.28522015 0.05376000 0.07559000 {++} 0.00000000 0 0 0 {?} >>{?} 129.19110107 0.40746999 0.64946997 {++} 0.00000000 0 0 0 {?} >> 13 0.071 0.000 0.000 0 2 {?} >>{?} 9.27318954 0.03744000 0.08241000 {++} 0.00000000 0 0 0 {?} >>{?} 125.45813751 0.36155999 0.66956002 {++} 0.00000000 0 0 0 {?} >> 14 0.062 0.000 0.000 0 2 {?} >>{?} 9.21533966 0.03507000 0.07084000 {++} 0.00000000 0 0 0 {?} >>{?} 129.98725891 0.29602000 0.73885000 {+P} 0.00000000 0 0 0 {?} >> 15 0.048 0.000 0.000 0 2 {?} >>{?} 9.19425964 0.03816000 0.09132000 {++} 0.00000000 0 0 0 {?} >>{?} 130.50273132 0.42578000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 16 0.094 0.000 0.000 0 2 {?} >>{?} 9.17389011 0.04072000 0.10156000 {++} 0.00000000 0 0 0 {?} >>{?} 127.68290710 0.35644999 0.67408001 {+P} 0.00000000 0 0 0 {?} >> 17 0.077 0.000 0.000 0 2 {?} >>{?} 9.17055035 0.03971000 0.08104000 {++} 0.00000000 0 0 0 {?} >>{?} 115.46961975 0.27941000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 18 0.056 0.000 0.000 0 2 {?} >>{?} 9.16213989 0.04747000 0.09716000 {++} 0.00000000 0 0 0 {?} >>{?} 114.84374237 0.22544999 0.74212003 {+P} 0.00000000 0 0 0 {?} >> 19 0.043 0.000 0.000 0 2 {?} >>{?} 9.15266991 0.05424000 0.14841001 {P+} 0.00000000 0 0 0 {?} >>{?} 128.36706543 0.37362999 1.03898001 {P+} 0.00000000 0 0 0 {?} >> 20 0.054 0.000 0.000 0 2 {?} >>{?} 9.15694046 0.04229000 0.08413000 {++} 0.00000000 0 0 0 {?} >>{?} 126.92595673 0.38988999 0.57476002 {++} 0.00000000 0 0 0 {?} >> 21 0.029 0.000 0.000 0 2 {?} >>{?} 9.10789013 0.04776000 0.07042000 {++} 0.00000000 0 0 0 {?} >>{?} 120.74434662 0.33715999 0.50563997 {++} 0.00000000 0 0 0 {?} >> 22 0.008 0.000 0.000 0 2 {?} >>{?} 9.07612991 0.02226000 0.02226000 {++} 0.00000000 0 0 0 {?} >>{?} 129.28369141 0.15385000 0.15386000 {++} 0.00000000 0 0 0 {?} >> 23 0.021 0.000 0.000 0 2 {?} >>{?} 9.07402992 0.03994000 0.05224000 {++} 0.00000000 0 0 0 {?} >>{?} 119.84877014 0.41582000 0.53865999 {++} 0.00000000 0 0 0 {?} >> 24 0.104 0.000 0.000 0 2 {?} >>{?} 9.07944012 0.03129000 0.07917000 {++} 0.00000000 0 0 0 {?} >>{?} 118.75666809 0.36021999 0.57981002 {++} 0.00000000 0 0 0 {?} >> 25 0.011 0.000 0.000 0 2 {?} >>{?} 9.06229019 0.02343000 0.05468000 {PP} 0.00000000 0 0 0 {?} >>{?} 128.39297485 0.43996000 0.37858000 {++} 0.00000000 0 0 0 {?} >> 26 0.045 0.000 0.000 0 2 {?} >>{?} 9.03810978 0.04700000 0.08043000 {++} 0.00000000 0 0 0 {?} >>{?} 124.52365112 0.31564000 0.56436998 {++} 0.00000000 0 0 0 {?} >> 27 0.012 0.000 0.000 0 2 {?} >>{?} 9.01138020 0.04522000 0.04324000 {++} 0.00000000 0 0 0 {?} >>{?} 122.77516937 0.59233999 0.57506001 {++} 0.00000000 0 0 0 {?} >> 28 0.020 0.000 0.000 0 2 {?} >>{?} 9.00827026 0.03905000 0.05669000 {+P} 0.00000000 0 0 0 {?} >>{?} 128.50689697 0.32813999 0.44837999 {++} 0.00000000 0 0 0 {?} >> 29 0.039 0.000 0.000 0 2 {?} >>{?} 8.98651981 0.04072000 0.08202000 {++} 0.00000000 0 0 0 {?} >>{?} 114.78943634 0.26657000 0.46957001 {++} 0.00000000 0 0 0 {?} >> 30 0.028 0.000 0.000 0 2 {?} >>{?} 8.97492027 0.06023000 0.08323000 {++} 0.00000000 0 0 0 {?} >>{?} 123.78687286 0.39003000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 31 0.028 0.000 0.000 0 2 {?} >>{?} 8.96115971 0.04479000 0.16403000 {P+} 0.00000000 0 0 0 {?} >>{?} 123.32784271 0.44527999 0.44527000 {+P} 0.00000000 0 0 0 {?} >> 32 0.028 0.000 0.000 0 2 {?} >>{?} 8.92486954 0.07565000 0.10456000 {++} 0.00000000 0 0 0 {?} >>{?} 122.50244904 0.31162000 0.48117000 {++} 0.00000000 0 0 0 {?} >> 33 0.012 0.000 0.000 0 2 {?} >>{?} 8.92082977 0.03513000 0.03240000 {++} 0.00000000 0 0 0 {?} >>{?} 121.73681641 0.40910000 0.38213000 {++} 0.00000000 0 0 0 {?} >> 34 0.049 0.000 0.000 0 2 {?} >>{?} 8.91040993 0.03644000 0.06716000 {++} 0.00000000 0 0 0 {?} >>{?} 117.42334747 0.35093999 0.56721002 {++} 0.00000000 0 0 0 {?} >> 35 0.009 0.000 0.000 0 2 {?} >>{?} 8.90561008 0.04431000 0.03194000 {++} 0.00000000 0 0 0 {?} >>{?} 120.65247345 0.45436001 0.34997001 {++} 0.00000000 0 0 0 {?} >> 36 0.052 0.000 0.000 0 2 {?} >>{?} 8.83215046 0.04029000 0.10374000 {P+} 0.00000000 0 0 0 {?} >>{?} 123.52065277 0.35095999 0.58156002 {++} 0.00000000 0 0 0 {?} >> 37 0.051 0.000 0.000 0 2 {?} >>{?} 8.83041000 0.04274000 0.09160000 {++} 0.00000000 0 0 0 {?} >>{?} 111.76838684 0.34373000 0.55707002 {++} 0.00000000 0 0 0 {?} >> 38 0.039 0.000 0.000 0 2 {?} >>{?} 8.81599998 0.05107000 0.10650000 {++} 0.00000000 0 0 0 {?} >>{?} 126.14125824 0.27833000 0.57964998 {++} 0.00000000 0 0 0 {?} >> 39 0.046 0.000 0.000 0 2 {?} >>{?} 8.81772041 0.04682000 0.08156000 {++} 0.00000000 0 0 0 {?} >>{?} 115.52069855 0.37502000 0.63911003 {++} 0.00000000 0 0 0 {?} >> 40 0.019 0.000 0.000 0 2 {?} >>{?} 8.79967976 0.04888000 0.06160000 {++} 0.00000000 0 0 0 {?} >>{?} 126.76438141 0.42118001 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 41 0.066 0.000 0.000 0 2 {?} >>{?} 8.80290031 0.04030000 0.08655000 {++} 0.00000000 0 0 0 {?} >>{?} 113.76141357 0.27004999 0.50932002 {++} 0.00000000 0 0 0 {?} >> 42 0.078 0.000 0.000 0 2 {?} >>{?} 8.79047012 0.03133000 0.08007000 {++} 0.00000000 0 0 0 {?} >>{?} 103.69535828 0.21854000 0.48743999 {++} 0.00000000 0 0 0 {?} >> 43 0.048 0.000 0.000 0 2 {?} >>{?} 8.78252029 0.05438000 0.08892000 {++} 0.00000000 0 0 0 {?} >>{?} 116.23068237 0.35815001 0.57308000 {++} 0.00000000 0 0 0 {?} >> 44 0.025 0.000 0.000 0 2 {?} >>{?} 8.76930046 0.05468000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 123.39900970 0.36063001 0.50209999 {++} 0.00000000 0 0 0 {?} >> 45 0.032 0.000 0.000 0 2 {?} >>{?} 8.74040031 0.04204000 0.06386000 {++} 0.00000000 0 0 0 {?} >>{?} 119.51757812 0.41496000 0.67391998 {++} 0.00000000 0 0 0 {?} >> 46 0.067 0.000 0.000 0 2 {?} >>{?} 8.73130989 0.04091000 0.08511000 {++} 0.00000000 0 0 0 {?} >>{?} 117.68920898 0.33182001 0.74212003 {P+} 0.00000000 0 0 0 {?} >> 47 0.060 0.000 0.000 0 2 {?} >>{?} 8.72500992 0.04861000 0.10378000 {++} 0.00000000 0 0 0 {?} >>{?} 117.16635132 0.35005999 0.58421999 {+P} 0.00000000 0 0 0 {?} >> 48 0.028 0.000 0.000 0 2 {?} >>{?} 8.68033981 0.05468000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 117.41108704 0.48805001 0.71780998 {++} 0.00000000 0 0 0 {?} >> 49 0.019 0.000 0.000 0 2 {?} >>{?} 8.66623974 0.03564000 0.04760000 {++} 0.00000000 0 0 0 {?} >>{?} 106.64694977 0.30864000 0.45392999 {++} 0.00000000 0 0 0 {?} >> 50 0.084 0.000 0.000 0 2 {?} >>{?} 8.66569042 0.03057000 0.10174000 {++} 0.00000000 0 0 0 {?} >>{?} 119.08283234 0.27796999 0.55557001 {++} 0.00000000 0 0 0 {?} >> 51 0.030 0.000 0.000 0 2 {?} >>{?} 8.62405968 0.03969000 0.05853000 {++} 0.00000000 0 0 0 {?} >>{?} 118.15601349 0.46595001 0.81713998 {++} 0.00000000 0 0 0 {?} >> 52 0.012 0.000 0.000 0 2 {?} >>{?} 8.60902977 0.02343000 0.04620000 {P+} 0.00000000 0 0 0 {?} >>{?} 124.81005096 0.49017000 0.47029001 {++} 0.00000000 0 0 0 {?} >> 53 0.010 0.000 0.000 0 2 {?} >>{?} 8.59885025 0.04310000 0.03356000 {++} 0.00000000 0 0 0 {?} >>{?} 114.46817017 0.48144999 0.39111999 {++} 0.00000000 0 0 0 {?} >> 54 0.037 0.000 0.000 0 2 {?} >>{?} 8.58979988 0.04240000 0.07690000 {P+} 0.00000000 0 0 0 {?} >>{?} 123.86728668 0.34246001 0.57284999 {++} 0.00000000 0 0 0 {?} >> 55 0.017 0.000 0.000 0 2 {?} >>{?} 8.58446026 0.04516000 0.05495000 {++} 0.00000000 0 0 0 {?} >>{?} 120.85059357 0.42071000 0.49362999 {++} 0.00000000 0 0 0 {?} >> 56 0.017 0.000 0.000 0 2 {?} >>{?} 8.56869030 0.04496000 0.05343000 {++} 0.00000000 0 0 0 {?} >>{?} 124.96684265 0.45776001 0.54070997 {++} 0.00000000 0 0 0 {?} >> 57 0.065 0.000 0.000 0 2 {?} >>{?} 8.56258965 0.03690000 0.08136000 {++} 0.00000000 0 0 0 {?} >>{?} 122.10099030 0.22215000 0.46597001 {++} 0.00000000 0 0 0 {?} >> 58 0.050 0.000 0.000 0 2 {?} >>{?} 8.56196976 0.04231000 0.09102000 {++} 0.00000000 0 0 0 {?} >>{?} 116.46385193 0.27871001 0.75085998 {++} 0.00000000 0 0 0 {?} >> 59 0.063 0.000 0.000 0 2 {?} >>{?} 8.55414963 0.04024000 0.08878000 {++} 0.00000000 0 0 0 {?} >>{?} 127.84677887 0.37467000 0.67422998 {++} 0.00000000 0 0 0 {?} >> 60 0.029 0.000 0.000 0 2 {?} >>{?} 8.53814030 0.05468000 0.14841001 {PP} 0.00000000 0 0 0 {?} >>{?} 123.95046234 0.45910001 0.69297999 {++} 0.00000000 0 0 0 {?} >> 61 0.025 0.000 0.000 0 2 {?} >>{?} 8.52645016 0.03905000 0.03905000 {+P} 0.00000000 0 0 0 {?} >>{?} 116.71658325 0.50573999 0.78671002 {++} 0.00000000 0 0 0 {?} >> 62 0.103 0.000 0.000 0 2 {?} >>{?} 8.50957012 0.03132000 0.16403000 {P+} 0.00000000 0 0 0 {?} >>{?} 119.74738312 0.25417000 0.57955003 {++} 0.00000000 0 0 0 {?} >> 63 0.015 0.000 0.000 0 2 {?} >>{?} 8.48196983 0.06846000 0.07540000 {++} 0.00000000 0 0 0 {?} >>{?} 121.43620300 0.43584999 0.47417000 {++} 0.00000000 0 0 0 {?} >> 64 0.033 0.000 0.000 0 2 {?} >>{?} 8.45549011 0.04476000 0.07118000 {++} 0.00000000 0 0 0 {?} >>{?} 122.88191223 0.28681999 0.47079000 {++} 0.00000000 0 0 0 {?} >> 65 0.037 0.000 0.000 0 2 {?} >>{?} 8.45928001 0.04884000 0.08407000 {++} 0.00000000 0 0 0 {?} >>{?} 111.97863770 0.24515000 0.46057001 {++} 0.00000000 0 0 0 {?} >> 66 0.053 0.000 0.000 0 2 {?} >>{?} 8.42555046 0.03763000 0.07183000 {++} 0.00000000 0 0 0 {?} >>{?} 130.45455933 0.28000000 0.54174000 {++} 0.00000000 0 0 0 {?} >> 67 0.070 0.000 0.000 0 2 {?} >>{?} 8.42586040 0.03709000 0.07706000 {++} 0.00000000 0 0 0 {?} >>{?} 123.67318726 0.34944001 0.56260002 {++} 0.00000000 0 0 0 {?} >> 68 0.103 0.000 0.000 0 2 {?} >>{?} 8.41983986 0.03891000 0.07494000 {++} 0.00000000 0 0 0 {?} >>{?} 125.46101379 0.28588000 0.52686000 {++} 0.00000000 0 0 0 {?} >> 69 0.078 0.000 0.000 0 2 {?} >>{?} 8.39888000 0.03397000 0.11716000 {P+} 0.00000000 0 0 0 {?} >>{?} 120.05713654 0.27757001 0.48684001 {++} 0.00000000 0 0 0 {?} >> 70 0.092 0.000 0.000 0 2 {?} >>{?} 8.38012981 0.03705000 0.09501000 {++} 0.00000000 0 0 0 {?} >>{?} 120.90222931 0.22251000 0.45534000 {++} 0.00000000 0 0 0 {?} >> 71 0.072 0.000 0.000 0 2 {?} >>{?} 8.34687996 0.03954000 0.08983000 {++} 0.00000000 0 0 0 {?} >>{?} 117.85575104 0.44801000 0.77595001 {++} 0.00000000 0 0 0 {?} >> 72 0.047 0.000 0.000 0 2 {?} >>{?} 8.33127975 0.03094000 0.07030000 {P+} 0.00000000 0 0 0 {?} >>{?} 122.21893311 0.32308000 0.51756001 {++} 0.00000000 0 0 0 {?} >> 73 0.033 0.000 0.000 0 2 {?} >>{?} 8.30879974 0.05318000 0.08187000 {++} 0.00000000 0 0 0 {?} >>{?} 123.27491760 0.33221999 0.52522999 {++} 0.00000000 0 0 0 {?} >> 74 0.134 0.000 0.000 0 2 {?} >>{?} 8.28635025 0.04634000 0.13279000 {PP} 0.00000000 0 0 0 {?} >>{?} 119.95139313 0.35797000 0.78309000 {P+} 0.00000000 0 0 0 {?} >> 75 0.068 0.000 0.000 0 2 {?} >>{?} 8.28258038 0.07030000 0.08592000 {PP} 0.00000000 0 0 0 {?} >>{?} 122.38706970 0.29898000 0.53735000 {++} 0.00000000 0 0 0 {?} >> 76 0.083 0.000 0.000 0 2 {?} >>{?} 8.27976990 0.03801000 0.07404000 {++} 0.00000000 0 0 0 {?} >>{?} 119.32097626 0.22105999 0.74212998 {PP} 0.00000000 0 0 0 {?} >> 77 0.074 0.000 0.000 0 2 {?} >>{?} 8.27359009 0.03553000 0.08592000 {P+} 0.00000000 0 0 0 {?} >>{?} 118.76410675 0.38033000 0.59671003 {+P} 0.00000000 0 0 0 {?} >> 78 0.072 0.000 0.000 0 2 {?} >>{?} 8.24851990 0.03926000 0.08821000 {++} 0.00000000 0 0 0 {?} >>{?} 125.80774689 0.26354000 0.55497998 {++} 0.00000000 0 0 0 {?} >> 79 0.146 0.000 0.000 0 2 {?} >>{?} 8.23853016 0.03098000 0.09021000 {++} 0.00000000 0 0 0 {?} >>{?} 123.59043121 0.20612000 0.49485001 {++} 0.00000000 0 0 0 {?} >> 80 0.041 0.000 0.000 0 2 {?} >>{?} 8.22673988 0.07561000 0.14841001 {P+} 0.00000000 0 0 0 {?} >>{?} 127.07125092 0.33230999 0.51292998 {++} 0.00000000 0 0 0 {?} >> 81 0.027 0.000 0.000 0 2 {?} >>{?} 8.21903038 0.05544000 0.09649000 {++} 0.00000000 0 0 0 {?} >>{?} 124.45092010 0.26997000 0.38450000 {++} 0.00000000 0 0 0 {?} >> 82 0.099 0.000 0.000 0 2 {?} >>{?} 8.21776962 0.03740000 0.13279000 {PP} 0.00000000 0 0 0 {?} >>{?} 122.48703766 0.33853999 0.55166000 {++} 0.00000000 0 0 0 {?} >> 83 0.036 0.000 0.000 0 2 {?} >>{?} 8.21453953 0.05468000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 119.88938141 0.37393999 0.53880000 {++} 0.00000000 0 0 0 {?} >> 84 0.064 0.000 0.000 0 2 {?} >>{?} 8.20197964 0.04460000 0.08623000 {++} 0.00000000 0 0 0 {?} >>{?} 120.80306244 0.29339999 0.49509001 {++} 0.00000000 0 0 0 {?} >> 85 0.062 0.000 0.000 0 2 {?} >>{?} 8.20011997 0.04328000 0.10154000 {+P} 0.00000000 0 0 0 {?} >>{?} 118.98993683 0.23966999 0.48096001 {++} 0.00000000 0 0 0 {?} >> 86 0.154 0.000 0.000 0 2 {?} >>{?} 8.19009972 0.05777000 0.15620001 {++} 0.00000000 0 0 0 {?} >>{?} 121.72383881 0.39014000 0.77187002 {++} 0.00000000 0 0 0 {?} >> 87 0.053 0.000 0.000 0 2 {?} >>{?} 8.15830994 0.03589000 0.06931000 {++} 0.00000000 0 0 0 {?} >>{?} 118.34718323 0.30368000 0.51214999 {+P} 0.00000000 0 0 0 {?} >> 88 0.040 0.000 0.000 0 2 {?} >>{?} 8.15443039 0.05547000 0.11072000 {++} 0.00000000 0 0 0 {?} >>{?} 115.29965973 0.28362000 0.50348002 {++} 0.00000000 0 0 0 {?} >> 89 0.013 0.000 0.000 0 2 {?} >>{?} 8.13809967 0.05795000 0.05731000 {++} 0.00000000 0 0 0 {?} >>{?} 111.16018677 0.41047999 0.40720999 {++} 0.00000000 0 0 0 {?} >> 90 0.106 0.000 0.000 0 2 {?} >>{?} 8.11168957 0.02982000 0.09589000 {+P} 0.00000000 0 0 0 {?} >>{?} 122.26255035 0.24295001 0.56563997 {++} 0.00000000 0 0 0 {?} >> 91 0.038 0.000 0.000 0 2 {?} >>{?} 8.10945034 0.05673000 0.12162000 {++} 0.00000000 0 0 0 {?} >>{?} 125.75801086 0.40685999 0.62101001 {++} 0.00000000 0 0 0 {?} >> 92 0.048 0.000 0.000 0 2 {?} >>{?} 8.09918976 0.05443000 0.11716000 {+P} 0.00000000 0 0 0 {?} >>{?} 127.07885742 0.36824000 0.55286002 {++} 0.00000000 0 0 0 {?} >> 93 0.011 0.000 0.000 0 2 {?} >>{?} 8.10035992 0.04359000 0.03708000 {++} 0.00000000 0 0 0 {?} >>{?} 123.18061066 0.45511001 0.39623001 {++} 0.00000000 0 0 0 {?} >> 94 0.023 0.000 0.000 0 2 {?} >>{?} 8.08104992 0.04719000 0.07092000 {++} 0.00000000 0 0 0 {?} >>{?} 127.96057892 0.48991999 0.62390000 {++} 0.00000000 0 0 0 {?} >> 95 0.032 0.000 0.000 0 2 {?} >>{?} 8.08753967 0.03432000 0.07558000 {++} 0.00000000 0 0 0 {?} >>{?} 112.05371857 0.38216999 0.59171999 {++} 0.00000000 0 0 0 {?} >> 96 0.024 0.000 0.000 0 2 {?} >>{?} 8.02731037 0.04671000 0.08505000 {++} 0.00000000 0 0 0 {?} >>{?} 109.40477753 0.42309001 0.53772998 {++} 0.00000000 0 0 0 {?} >> 97 0.013 0.000 0.000 0 2 {?} >>{?} 8.00454044 0.04723000 0.04808000 {++} 0.00000000 0 0 0 {?} >>{?} 132.23956299 0.33691999 0.34106001 {++} 0.00000000 0 0 0 {?} >> 98 0.090 0.000 0.000 0 2 {?} >>{?} 8.00611973 0.04411000 0.09238000 {++} 0.00000000 0 0 0 {?} >>{?} 114.71705627 0.30535001 0.73027998 {++} 0.00000000 0 0 0 {?} >> 99 0.069 0.000 0.000 0 2 {?} >>{?} 7.97673988 0.03751000 0.09519000 {++} 0.00000000 0 0 0 {?} >>{?} 120.48632050 0.24705000 0.51012999 {++} 0.00000000 0 0 0 {?} >> 100 0.034 0.000 0.000 0 2 {?} >>{?} 7.97504997 0.05403000 0.08892000 {++} 0.00000000 0 0 0 {?} >>{?} 115.63549805 0.49608999 0.73193997 {++} 0.00000000 0 0 0 {?} >> 101 0.108 0.000 0.000 0 2 {?} >>{?} 7.94001007 0.03134000 0.07565000 {++} 0.00000000 0 0 0 {?} >>{?} 118.79782867 0.26848999 0.55167001 {++} 0.00000000 0 0 0 {?} >> 102 0.010 0.000 0.000 0 2 {?} >>{?} 7.93320990 0.02439000 0.05468000 {P+} 0.00000000 0 0 0 {?} >>{?} 119.38912201 0.44527000 0.64958000 {P+} 0.00000000 0 0 0 {?} >> 103 0.115 0.000 0.000 0 2 {?} >>{?} 7.92363977 0.02922000 0.08967000 {++} 0.00000000 0 0 0 {?} >>{?} 122.06256866 0.27302000 0.57780999 {++} 0.00000000 0 0 0 {?} >> 104 0.091 0.000 0.000 0 2 {?} >>{?} 7.92298985 0.03373000 0.09724000 {++} 0.00000000 0 0 0 {?} >>{?} 110.10894775 0.24812999 0.54105997 {++} 0.00000000 0 0 0 {?} >> 105 0.034 0.000 0.000 0 2 {?} >>{?} 7.91328001 0.05084000 0.11716000 {P+} 0.00000000 0 0 0 {?} >>{?} 114.27411652 0.31005999 0.51721001 {++} 0.00000000 0 0 0 {?} >> 106 0.044 0.000 0.000 0 2 {?} >>{?} 7.91203022 0.05017000 0.09908000 {++} 0.00000000 0 0 0 {?} >>{?} 106.12254333 0.29020000 0.52490997 {++} 0.00000000 0 0 0 {?} >> 107 0.067 0.000 0.000 0 2 {?} >>{?} 7.89022017 0.03946000 0.08243000 {++} 0.00000000 0 0 0 {?} >>{?} 108.95504761 0.34522000 0.59619999 {++} 0.00000000 0 0 0 {?} >> 108 0.035 0.000 0.000 0 2 {?} >>{?} 7.86790991 0.05643000 0.09543000 {++} 0.00000000 0 0 0 {?} >>{?} 118.04812622 0.38444999 0.54345000 {++} 0.00000000 0 0 0 {?} >> 109 0.069 0.000 0.000 0 2 {?} >>{?} 7.86463022 0.05152000 0.11392000 {++} 0.00000000 0 0 0 {?} >>{?} 116.64164734 0.26468000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 110 0.113 0.000 0.000 0 2 {?} >>{?} 7.86288977 0.02343000 0.10701000 {P+} 0.00000000 0 0 0 {?} >>{?} 116.13739014 0.26254001 0.57420999 {+P} 0.00000000 0 0 0 {?} >> 111 0.114 0.000 0.000 0 2 {?} >>{?} 7.83620977 0.05468000 0.07030000 {PP} 0.00000000 0 0 0 {?} >>{?} 116.16040802 0.29398000 0.59298003 {++} 0.00000000 0 0 0 {?} >> 112 0.011 0.000 0.000 0 2 {?} >>{?} 7.83151007 0.05468000 0.05026000 {+P} 0.00000000 0 0 0 {?} >>{?} 114.34314728 0.36722001 0.32308999 {++} 0.00000000 0 0 0 {?} >> 113 0.075 0.000 0.000 0 2 {?} >>{?} 7.82917023 0.03508000 0.09460000 {++} 0.00000000 0 0 0 {?} >>{?} 119.80609131 0.41453001 0.79957002 {P+} 0.00000000 0 0 0 {?} >> 114 0.133 0.000 0.000 0 2 {?} >>{?} 7.81687021 0.02841000 0.06243000 {++} 0.00000000 0 0 0 {?} >>{?} 112.86757660 0.23194000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 115 0.096 0.000 0.000 0 2 {?} >>{?} 7.79023981 0.03768000 0.22652000 {PP} 0.00000000 0 0 0 {?} >>{?} 119.09896088 0.34018999 0.58897001 {++} 0.00000000 0 0 0 {?} >> 116 0.064 0.000 0.000 0 2 {?} >>{?} 7.78104019 0.04095000 0.08962000 {++} 0.00000000 0 0 0 {?} >>{?} 121.07984161 0.24089999 0.55251998 {++} 0.00000000 0 0 0 {?} >> 117 0.114 0.000 0.000 0 2 {?} >>{?} 7.77900982 0.03997000 0.14841001 {PP} 0.00000000 0 0 0 {?} >>{?} 115.99224091 0.23217000 0.52179003 {+P} 0.00000000 0 0 0 {?} >> 118 0.080 0.000 0.000 0 2 {?} >>{?} 7.77311993 0.04597000 0.11716000 {P+} 0.00000000 0 0 0 {?} >>{?} 111.73473358 0.21788999 0.51991999 {++} 0.00000000 0 0 0 {?} >> 119 0.382 0.000 0.000 0 2 {?} >>{?} 7.71002007 0.02754000 0.05970000 {++} 0.00000000 0 0 0 {?} >>{?} 129.99447632 0.19433001 0.51626998 {++} 0.00000000 0 0 0 {?} >> 120 0.045 0.000 0.000 0 2 {?} >>{?} 7.68874979 0.03097000 0.07452000 {P+} 0.00000000 0 0 0 {?} >>{?} 122.33661652 0.39862001 0.58831000 {++} 0.00000000 0 0 0 {?} >> 121 0.271 0.000 0.000 0 2 {?} >>{?} 7.68454981 0.02787000 0.06094000 {++} 0.00000000 0 0 0 {?} >>{?} 111.95554352 0.24741000 0.56757998 {++} 0.00000000 0 0 0 {?} >> 122 0.119 0.000 0.000 0 2 {?} >>{?} 7.65936995 0.02691000 0.06044000 {++} 0.00000000 0 0 0 {?} >>{?} 114.28424835 0.25543001 1.03898001 {P+} 0.00000000 0 0 0 {?} >> 123 0.080 0.000 0.000 0 2 {?} >>{?} 7.65795994 0.02919000 0.11716000 {P+} 0.00000000 0 0 0 {?} >>{?} 121.18952179 0.23035000 0.48798999 {++} 0.00000000 0 0 0 {?} >> 124 0.017 0.000 0.000 0 2 {?} >>{?} 7.64488983 0.05116000 0.06227000 {++} 0.00000000 0 0 0 {?} >>{?} 119.21913147 0.48416001 0.54899001 {++} 0.00000000 0 0 0 {?} >> 125 0.076 0.000 0.000 0 2 {?} >>{?} 7.63647985 0.03655000 0.07383000 {++} 0.00000000 0 0 0 {?} >>{?} 110.58168793 0.29012001 0.58112001 {++} 0.00000000 0 0 0 {?} >> 126 0.051 0.000 0.000 0 2 {?} >>{?} 7.63299990 0.02872000 0.06046000 {+P} 0.00000000 0 0 0 {?} >>{?} 122.31163788 0.34492999 0.58973002 {++} 0.00000000 0 0 0 {?} >> 127 0.116 0.000 0.000 0 2 {?} >>{?} 7.60082006 0.02880000 0.06893000 {++} 0.00000000 0 0 0 {?} >>{?} 112.74240112 0.21319000 0.56378001 {+P} 0.00000000 0 0 0 {?} >> 128 0.062 0.000 0.000 0 2 {?} >>{?} 7.59600019 0.03667000 0.07325000 {P+} 0.00000000 0 0 0 {?} >>{?} 112.08483124 0.37825999 0.56854999 {++} 0.00000000 0 0 0 {?} >> 129 0.078 0.000 0.000 0 2 {?} >>{?} 7.59168005 0.04196000 0.12372000 {P+} 0.00000000 0 0 0 {?} >>{?} 120.47145081 0.24133000 0.58583999 {++} 0.00000000 0 0 0 {?} >> 130 0.010 0.000 0.000 0 2 {?} >>{?} 7.59217978 0.04007000 0.03435000 {++} 0.00000000 0 0 0 {?} >>{?} 118.49476624 0.40586999 0.33515999 {++} 0.00000000 0 0 0 {?} >> 131 0.073 0.000 0.000 0 2 {?} >>{?} 7.56899977 0.03887000 0.08929000 {++} 0.00000000 0 0 0 {?} >>{?} 113.17603302 0.23255000 0.50026000 {++} 0.00000000 0 0 0 {?} >> 132 0.014 0.000 0.000 0 2 {?} >>{?} 7.56336021 0.02765000 0.03047000 {+P} 0.00000000 0 0 0 {?} >>{?} 112.57707214 0.08950000 0.09794000 {N+} 0.00000000 0 0 0 {?} >> 133 0.112 0.000 0.000 0 2 {?} >>{?} 7.56378984 0.02965000 0.07362000 {++} 0.00000000 0 0 0 {?} >>{?} 111.95867157 0.30838001 0.60839999 {++} 0.00000000 0 0 0 {?} >> 134 0.009 0.000 0.000 0 2 {?} >>{?} 7.55337000 0.01987000 0.01987000 {++} 0.00000000 0 0 0 {?} >>{?} 115.73932648 0.28731000 0.28731000 {++} 0.00000000 0 0 0 {?} >> 135 0.016 0.000 0.000 0 2 {?} >>{?} 7.55341005 0.07461000 0.08289000 {++} 0.00000000 0 0 0 {?} >>{?} 111.18615723 0.46373001 0.52023000 {++} 0.00000000 0 0 0 {?} >> 136 0.050 0.000 0.000 0 2 {?} >>{?} 7.53483009 0.04818000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 120.61028290 0.26271999 0.48480001 {++} 0.00000000 0 0 0 {?} >> 137 0.047 0.000 0.000 0 2 {?} >>{?} 7.50721979 0.03964000 0.09295000 {P+} 0.00000000 0 0 0 {?} >>{?} 116.81124878 0.32414001 0.56163001 {++} 0.00000000 0 0 0 {?} >> 138 0.023 0.000 0.000 0 2 {?} >>{?} 7.47169018 0.04238000 0.06207000 {P+} 0.00000000 0 0 0 {?} >>{?} 121.83750153 0.32451999 0.45300999 {++} 0.00000000 0 0 0 {?} >> 139 0.099 0.000 0.000 0 2 {?} >>{?} 7.47609997 0.03320000 0.07579000 {++} 0.00000000 0 0 0 {?} >>{?} 119.60140228 0.25848001 0.55805999 {++} 0.00000000 0 0 0 {?} >> 140 0.064 0.000 0.000 0 2 {?} >>{?} 7.43861008 0.05132000 0.12446000 {++} 0.00000000 0 0 0 {?} >>{?} 116.54441833 0.49568999 1.08117998 {P+} 0.00000000 0 0 0 {?} >> 141 0.023 0.000 0.000 0 2 {?} >>{?} 7.42959976 0.04075000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 121.82862091 0.29200000 0.42462999 {++} 0.00000000 0 0 0 {?} >> 142 0.032 0.000 0.000 0 2 {?} >>{?} 7.41245985 0.05225000 0.10267000 {++} 0.00000000 0 0 0 {?} >>{?} 113.31770325 0.37788999 0.56540000 {++} 0.00000000 0 0 0 {?} >> 143 0.060 0.000 0.000 0 2 {?} >>{?} 7.41304016 0.03960000 0.08664000 {++} 0.00000000 0 0 0 {?} >>{?} 108.34221649 0.24741000 0.53959000 {++} 0.00000000 0 0 0 {?} >> 144 0.221 0.000 0.000 0 2 {?} >>{?} 7.40110016 0.02917000 0.09772000 {++} 0.00000000 0 0 0 {?} >>{?} 118.17514801 0.35451999 0.84536999 {++} 0.00000000 0 0 0 {?} >> 145 0.026 0.000 0.000 0 2 {?} >>{?} 7.40603018 0.04686000 0.07549000 {++} 0.00000000 0 0 0 {?} >>{?} 116.97888947 0.39438000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 146 0.124 0.000 0.000 0 2 {?} >>{?} 7.40754986 0.04023000 0.19527000 {P+} 0.00000000 0 0 0 {?} >>{?} 116.12361908 0.37531999 0.61923999 {+P} 0.00000000 0 0 0 {?} >> 147 0.063 0.000 0.000 0 2 {?} >>{?} 7.39592981 0.03555000 0.07429000 {++} 0.00000000 0 0 0 {?} >>{?} 111.55667114 0.33074000 0.79591000 {++} 0.00000000 0 0 0 {?} >> 148 0.087 0.000 0.000 0 2 {?} >>{?} 7.35832024 0.04036000 0.10146000 {++} 0.00000000 0 0 0 {?} >>{?} 119.92883301 0.27529001 0.58060998 {++} 0.00000000 0 0 0 {?} >> 149 0.009 0.000 0.000 0 2 {?} >>{?} 7.34241009 0.02205000 0.02205000 {++} 0.00000000 0 0 0 {?} >>{?} 122.07758331 0.18825001 0.18825001 {++} 0.00000000 0 0 0 {?} >> 150 0.014 0.000 0.000 0 2 {?} >>{?} 7.29853010 0.03149000 0.03417000 {++} 0.00000000 0 0 0 {?} >>{?} 112.27043915 0.29628000 0.32751000 {++} 0.00000000 0 0 0 {?} >> 151 0.073 0.000 0.000 0 2 {?} >>{?} 7.29853010 0.03188000 0.06641000 {++} 0.00000000 0 0 0 {?} >>{?} 99.90215302 0.33442000 0.60668999 {++} 0.00000000 0 0 0 {?} >> 152 0.015 0.000 0.000 0 2 {?} >>{?} 7.25656986 0.07310000 0.07816000 {++} 0.00000000 0 0 0 {?} >>{?} 123.37146759 0.45230001 0.49380001 {++} 0.00000000 0 0 0 {?} >> 153 0.029 0.000 0.000 0 2 {?} >>{?} 7.25699997 0.05468000 0.10500000 {P+} 0.00000000 0 0 0 {?} >>{?} 122.11892700 0.27245000 0.46195999 {++} 0.00000000 0 0 0 {?} >> 154 0.061 0.000 0.000 0 2 {?} >>{?} 7.25499010 0.04322000 0.07692000 {++} 0.00000000 0 0 0 {?} >>{?} 118.87946320 0.25835001 0.51672000 {++} 0.00000000 0 0 0 {?} >> 155 0.062 0.000 0.000 0 2 {?} >>{?} 7.25256014 0.02981000 0.05918000 {++} 0.00000000 0 0 0 {?} >>{?} 109.41586304 0.35773000 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 156 0.036 0.000 0.000 0 2 {?} >>{?} 7.20282984 0.03937000 0.07030000 {+P} 0.00000000 0 0 0 {?} >>{?} 122.14833069 0.26865000 0.49294999 {++} 0.00000000 0 0 0 {?} >> 157 0.060 0.000 0.000 0 2 {?} >>{?} 7.15799999 0.03602000 0.07567000 {++} 0.00000000 0 0 0 {?} >>{?} 124.59234619 0.24829000 0.50958002 {++} 0.00000000 0 0 0 {?} >> 158 0.108 0.000 0.000 0 2 {?} >>{?} 7.10200977 0.03328000 0.07760000 {++} 0.00000000 0 0 0 {?} >>{?} 121.29873657 0.28959000 0.55466002 {++} 0.00000000 0 0 0 {?} >> 159 0.012 0.000 0.000 0 2 {?} >>{?} 7.08515978 0.03102000 0.03102000 {++} 0.00000000 0 0 0 {?} >>{?} 113.41272736 0.51080000 0.46746999 {++} 0.00000000 0 0 0 {?} >> 160 0.057 0.000 0.000 0 2 {?} >>{?} 7.08311987 0.03451000 0.06392000 {++} 0.00000000 0 0 0 {?} >>{?} 111.07150269 0.36837000 0.78763998 {++} 0.00000000 0 0 0 {?} >> 161 0.104 0.000 0.000 0 2 {?} >>{?} 7.06606007 0.03267000 0.11041000 {++} 0.00000000 0 0 0 {?} >>{?} 121.98676300 0.23470999 0.56619000 {++} 0.00000000 0 0 0 {?} >> 162 0.231 0.000 0.000 0 2 {?} >>{?} 7.00230980 0.02600000 0.05954000 {++} 0.00000000 0 0 0 {?} >>{?} 111.96074677 0.23773000 0.56208003 {++} 0.00000000 0 0 0 {?} >> 163 0.063 0.000 0.000 0 2 {?} >>{?} 6.98186016 0.04768000 0.09240000 {++} 0.00000000 0 0 0 {?} >>{?} 116.69972229 0.38938999 0.75615001 {++} 0.00000000 0 0 0 {?} >> 164 0.118 0.000 0.000 0 2 {?} >>{?} 6.97740984 0.02784000 0.06242000 {++} 0.00000000 0 0 0 {?} >>{?} 114.28914642 0.25237000 1.03898001 {P+} 0.00000000 0 0 0 {?} >> 165 0.045 0.000 0.000 0 2 {?} >>{?} 6.94825983 0.04288000 0.12067000 {++} 0.00000000 0 0 0 {?} >>{?} 116.37777710 0.44916001 0.65894997 {++} 0.00000000 0 0 0 {?} >> 166 0.113 0.000 0.000 0 2 {?} >>{?} 6.92364979 0.03855000 0.07815000 {P+} 0.00000000 0 0 0 {?} >>{?} 112.74288177 0.21718000 0.58090001 {++} 0.00000000 0 0 0 {?} >> 167 0.157 0.000 0.000 0 2 {?} >>{?} 6.88015985 0.03658000 0.05468000 {+P} 0.00000000 0 0 0 {?} >>{?} 112.85703278 0.24023999 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 168 0.057 0.000 0.000 0 2 {?} >>{?} 6.76773977 0.03415000 0.07223000 {++} 0.00000000 0 0 0 {?} >>{?} 109.39920044 0.30996001 0.74212998 {P+} 0.00000000 0 0 0 {?} >> 169 0.024 0.000 0.000 0 2 {?} >>{?} 6.76249981 0.04589000 0.06563000 {++} 0.00000000 0 0 0 {?} >>{?} 117.41477203 0.43112999 0.58424002 {++} 0.00000000 0 0 0 {?} >> 170 0.075 0.000 0.000 0 2 {?} >>{?} 6.76338005 0.03969000 0.12415000 {P+} 0.00000000 0 0 0 {?} >>{?} 111.54160309 0.28996000 0.72551000 {+P} 0.00000000 0 0 0 {?} >> 171 0.020 0.000 0.000 0 2 {?} >>{?} 6.71824980 0.05397000 0.06661000 {++} 0.00000000 0 0 0 {?} >>{?} 119.68673706 0.45320001 0.61105001 {++} 0.00000000 0 0 0 {?} >> 172 0.018 0.000 0.000 0 2 {?} >>{?} 6.71492004 0.03788000 0.03905000 {+P} 0.00000000 0 0 0 {?} >>{?} 111.38577271 0.24659000 0.32400000 {++} 0.00000000 0 0 0 {?} >> 173 0.186 0.000 0.000 0 2 {?} >>{?} 6.70755005 0.03075000 0.06890000 {+P} 0.00000000 0 0 0 {?} >>{?} 111.95716095 0.25158000 0.56826001 {++} 0.00000000 0 0 0 {?} >> 174 0.037 0.000 0.000 0 2 {?} >>{?} 6.66259003 0.04336000 0.10154000 {P+} 0.00000000 0 0 0 {?} >>{?} 113.98639679 0.38521001 0.58822000 {++} 0.00000000 0 0 0 {?} >> 175 0.071 0.000 0.000 0 2 {?} >>{?} 6.52921009 0.04400000 0.08558000 {++} 0.00000000 0 0 0 {?} >>{?} 115.65345001 0.36008999 0.61123002 {++} 0.00000000 0 0 0 {?} >> 176 0.018 0.000 0.000 0 2 {?} >>{?} 6.35503006 0.05859000 0.07234000 {++} 0.00000000 0 0 0 {?} >>{?} 120.23181915 0.35025999 0.45297000 {++} 0.00000000 0 0 0 {?} >> 177 0.020 0.000 0.000 0 2 {?} >>{?} 6.20161009 0.04460000 0.06079000 {++} 0.00000000 0 0 0 {?} >>{?} 108.81668854 0.35619000 0.44850001 {++} 0.00000000 0 0 0 {?} >> >>stop_ >>; >> >> loop_ >> _Spectral_dim.ID >> _Spectral_dim.Atom_type >> _Spectral_dim.Atom_isotope_number >> _Spectral_dim.Spectral_region >> _Spectral_dim.Magnetization_linkage_ID >> _Spectral_dim.Sweep_width >> _Spectral_dim.Sweep_width_units >> _Spectral_dim.Encoding_code >> _Spectral_dim.Encoded_source_dimension_ID >> _Spectral_dim.Entry_ID >> _Spectral_dim.Spectral_peak_list_ID >> >> 2 H 1 H . 7682 . . . 16669 1 >> 2 N 15 N . 2293 . . . 16669 1 >> >> stop_ >> >> loop_ >> _Spectral_peak_software.Software_ID >> _Spectral_peak_software.Software_label >> _Spectral_peak_software.Method_ID >> _Spectral_peak_software.Method_label >> _Spectral_peak_software.Entry_ID >> _Spectral_peak_software.Spectral_peak_list_ID >> >> 1 $NMRView . . 16669 1 >> >> stop_ >> >>save_ >> ; save_