data_10018 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 10018 _Entry.Title ; 1H Chemical Shift Assignments for LINE RNA ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2005-12-14 _Entry.Accession_date 2005-12-14 _Entry.Last_release_date 2006-11-21 _Entry.Original_release_date 2006-11-21 _Entry.Origination author _Entry.NMR_STAR_version 3.1.1.61 _Entry.Original_NMR_STAR_version . _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.Entry_ID 1 Yusuke Nomura . . . 10018 2 Seiki Baba . . . 10018 3 Shinta Nakazato . . . 10018 4 Taiichi Sakamoto . . . 10018 5 Masaki Kajikawa . . . 10018 6 Norihiro Okada . . . 10018 7 Gota Kawai . . . 10018 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 10018 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '1H chemical shifts' 178 10018 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2006-11-21 2005-12-14 original author . 10018 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID PDB 2FDT 'BMRB Entry Tracking System' 10018 stop_ save_ ############### # Citations # ############### save_citiation_1 _Citation.Sf_category citations _Citation.Sf_framecode citiation_1 _Citation.Entry_ID 10018 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 17000640 _Citation.Full_citation . _Citation.Title 'Solution structure and functional importance of a conserved RNA hairpin of eel LINE UnaL2' _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Nucleic Acids Res.' _Citation.Journal_name_full . _Citation.Journal_volume 34 _Citation.Journal_issue 18 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 5184 _Citation.Page_last 5193 _Citation.Year 2006 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Yusuke Nomura . . . 10018 1 2 Masaki Kajikawa . . . 10018 1 3 Seiki Baba . . . 10018 1 4 Shinta Nakazato . . . 10018 1 5 T. Imai . . . 10018 1 6 Taiichi Sakamoto . . . 10018 1 7 Norihiro Okada . . . 10018 1 8 Gota Kawai . . . 10018 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 10018 _Assembly.ID 1 _Assembly.Name 'RNA hairpin of eel LINE' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites no _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state 'not present' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Assembly_type.Type _Assembly_type.Entry_ID _Assembly_type.Assembly_ID 'RNA single strand' 10018 1 stop_ loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'RNA hairpin of eel LINE' 1 $LINE36 . . yes native no no . . . 10018 1 stop_ loop_ _Assembly_db_link.Author_supplied _Assembly_db_link.Database_code _Assembly_db_link.Accession_code _Assembly_db_link.Entry_mol_code _Assembly_db_link.Entry_mol_name _Assembly_db_link.Entry_experimental_method _Assembly_db_link.Entry_structure_resolution _Assembly_db_link.Entry_relation_type _Assembly_db_link.Entry_details _Assembly_db_link.Entry_ID _Assembly_db_link.Assembly_ID yes PDB 2FDT . . . . . . 10018 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_LINE36 _Entity.Sf_category entity _Entity.Sf_framecode LINE36 _Entity.Entry_ID 10018 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name LINE36 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GGUUGUACGUCGCUUUGGAU AAAAGCGUCUGCGACC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 36 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . G . 10018 1 2 . G . 10018 1 3 . U . 10018 1 4 . U . 10018 1 5 . G . 10018 1 6 . U . 10018 1 7 . A . 10018 1 8 . C . 10018 1 9 . G . 10018 1 10 . U . 10018 1 11 . C . 10018 1 12 . G . 10018 1 13 . C . 10018 1 14 . U . 10018 1 15 . U . 10018 1 16 . U . 10018 1 17 . G . 10018 1 18 . G . 10018 1 19 . A . 10018 1 20 . U . 10018 1 21 . A . 10018 1 22 . A . 10018 1 23 . A . 10018 1 24 . A . 10018 1 25 . G . 10018 1 26 . C . 10018 1 27 . G . 10018 1 28 . U . 10018 1 29 . C . 10018 1 30 . U . 10018 1 31 . G . 10018 1 32 . C . 10018 1 33 . G . 10018 1 34 . A . 10018 1 35 . C . 10018 1 36 . C . 10018 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 10018 1 . G 2 2 10018 1 . U 3 3 10018 1 . U 4 4 10018 1 . G 5 5 10018 1 . U 6 6 10018 1 . A 7 7 10018 1 . C 8 8 10018 1 . G 9 9 10018 1 . U 10 10 10018 1 . C 11 11 10018 1 . G 12 12 10018 1 . C 13 13 10018 1 . U 14 14 10018 1 . U 15 15 10018 1 . U 16 16 10018 1 . G 17 17 10018 1 . G 18 18 10018 1 . A 19 19 10018 1 . U 20 20 10018 1 . A 21 21 10018 1 . A 22 22 10018 1 . A 23 23 10018 1 . A 24 24 10018 1 . G 25 25 10018 1 . C 26 26 10018 1 . G 27 27 10018 1 . U 28 28 10018 1 . C 29 29 10018 1 . U 30 30 10018 1 . G 31 31 10018 1 . C 32 32 10018 1 . G 33 33 10018 1 . A 34 34 10018 1 . C 35 35 10018 1 . C 36 36 10018 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 10018 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Subvariant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Cellular_location _Entity_natural_src.Fragment _Entity_natural_src.Fraction _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Plasmid_details _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Dev_stage _Entity_natural_src.Details _Entity_natural_src.Citation_ID _Entity_natural_src.Citation_label _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $LINE36 . 7937 . . . 'Japanese eel' . . Eukaryota Metazoa Anguilla Japonica . . . . . . . . . . . . . . . . . . . . . 10018 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 10018 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_subvariant _Entity_experimental_src.Host_org_organ _Entity_experimental_src.Host_org_tissue _Entity_experimental_src.Host_org_tissue_fraction _Entity_experimental_src.Host_org_cell_line _Entity_experimental_src.Host_org_cell_type _Entity_experimental_src.Host_org_cellular_location _Entity_experimental_src.Host_org_organelle _Entity_experimental_src.Host_org_gene _Entity_experimental_src.Host_org_culture_collection _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Host_org_dev_stage _Entity_experimental_src.Details _Entity_experimental_src.Citation_ID _Entity_experimental_src.Citation_label _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $LINE36 . 'enzymatic synthesis' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10018 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 10018 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 LINE36 . . . 1 $LINE36 . . 1.0 . . mM 0.1 . . . 10018 1 stop_ save_ ####################### # Sample conditions # ####################### save_condition_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode condition_1 _Sample_condition_list.Entry_ID 10018 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.0 0.1 pH 10018 1 temperature 293 0.1 K 10018 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_600MHz_spectrometer _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode 600MHz_spectrometer _NMR_spectrometer.Entry_ID 10018 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_500MHz_spectrometer _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode 500MHz_spectrometer _NMR_spectrometer.Entry_ID 10018 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 500 save_ ############################# # NMR applied experiments # ############################# save_NMR_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode NMR_experiment_list _Experiment_list.Entry_ID 10018 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D NOESY' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 2 '2D TOCSY' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 3 DQF-COSY no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 4 HP-COSY no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 2 $500MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 5 HCP no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 2 $500MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 6 'HALF FILTERED NOESY' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 7 '2D HNN-COSY' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 8 '2D HSQC' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 9 '2D TROSY' no . . . . . . . . . . 1 $sample_1 . . . 1 $condition_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 10018 1 stop_ save_ save_2D_NOESY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode 2D_NOESY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 1 _NMR_spec_expt.Name '2D NOESY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_2D_TOCSY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode 2D_TOCSY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 2 _NMR_spec_expt.Name '2D TOCSY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_DQF-COSY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode DQF-COSY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 3 _NMR_spec_expt.Name DQF-COSY _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_HP-COSY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode HP-COSY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 4 _NMR_spec_expt.Name HP-COSY _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 2 _NMR_spec_expt.NMR_spectrometer_label $500MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_HCP _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode HCP _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 5 _NMR_spec_expt.Name HCP _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 2 _NMR_spec_expt.NMR_spectrometer_label $500MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_HALF_FILTERED_NOESY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode HALF_FILTERED_NOESY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 6 _NMR_spec_expt.Name 'HALF FILTERED NOESY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_2D_HNN-COSY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode 2D_HNN-COSY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 7 _NMR_spec_expt.Name '2D HNN-COSY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_2D_HSQC _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode 2D_HSQC _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 8 _NMR_spec_expt.Name '2D HSQC' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ save_2D_TROSY _NMR_spec_expt.Sf_category NMR_spectrometer_expt _NMR_spec_expt.Sf_framecode 2D_TROSY _NMR_spec_expt.Entry_ID 10018 _NMR_spec_expt.ID 9 _NMR_spec_expt.Name '2D TROSY' _NMR_spec_expt.Type . _NMR_spec_expt.Sample_volume . _NMR_spec_expt.Sample_volume_units . _NMR_spec_expt.NMR_tube_type . _NMR_spec_expt.Sample_spinning_rate . _NMR_spec_expt.Sample_angle . _NMR_spec_expt.NMR_spectrometer_ID 1 _NMR_spec_expt.NMR_spectrometer_label $600MHz_spectrometer _NMR_spec_expt.NMR_spectrometer_probe_ID . _NMR_spec_expt.NMR_spectrometer_probe_label . _NMR_spec_expt.Carrier_freq_switch_time . _NMR_spec_expt.Software_ID . _NMR_spec_expt.Software_label . _NMR_spec_expt.Method_ID . _NMR_spec_expt.Method_label . _NMR_spec_expt.Pulse_seq_accession_BMRB_code . _NMR_spec_expt.Details . save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_Chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode Chem_shift_reference_1 _Chem_shift_reference.Entry_ID 10018 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Indirect_shift_ratio_cit_ID _Chem_shift_ref.Indirect_shift_ratio_cit_label _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Correction_val_cit_ID _Chem_shift_ref.Correction_val_cit_label _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . ppm 0.0 internal direct 1.0 . . . . . . . . . 10018 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_L36 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode L36 _Assigned_chem_shift_list.Entry_ID 10018 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $condition_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $Chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D NOESY' 1 $sample_1 isotropic 10018 1 2 '2D TOCSY' 1 $sample_1 isotropic 10018 1 3 DQF-COSY 1 $sample_1 isotropic 10018 1 4 HP-COSY 1 $sample_1 isotropic 10018 1 5 HCP 1 $sample_1 isotropic 10018 1 6 'HALF FILTERED NOESY' 1 $sample_1 isotropic 10018 1 7 '2D HNN-COSY' 1 $sample_1 isotropic 10018 1 8 '2D HSQC' 1 $sample_1 isotropic 10018 1 9 '2D TROSY' 1 $sample_1 isotropic 10018 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 G H8 H 1 8.145 0.02 . 1 . . . . 1 G H8 . 10018 1 2 . 1 1 1 1 G H1' H 1 5.822 0.02 . 1 . . . . 1 G H1' . 10018 1 3 . 1 1 1 1 G H2' H 1 4.957 0.02 . 1 . . . . 1 G H2' . 10018 1 4 . 1 1 1 1 G H3' H 1 4.699 0.02 . 1 . . . . 1 G H3' . 10018 1 5 . 1 1 2 2 G H8 H 1 7.542 0.02 . 1 . . . . 2 G H8 . 10018 1 6 . 1 1 2 2 G H1' H 1 5.936 0.02 . 1 . . . . 2 G H1' . 10018 1 7 . 1 1 2 2 G H2' H 1 4.569 0.02 . 1 . . . . 2 G H2' . 10018 1 8 . 1 1 3 3 U H5 H 1 5.111 0.02 . 1 . . . . 3 U H5 . 10018 1 9 . 1 1 3 3 U H6 H 1 7.641 0.02 . 1 . . . . 3 U H6 . 10018 1 10 . 1 1 3 3 U H1' H 1 5.581 0.02 . 1 . . . . 3 U H1' . 10018 1 11 . 1 1 3 3 U H2' H 1 4.667 0.02 . 1 . . . . 3 U H2' . 10018 1 12 . 1 1 3 3 U H3' H 1 4.376 0.02 . 1 . . . . 3 U H3' . 10018 1 13 . 1 1 3 3 U H4' H 1 4.461 0.02 . 1 . . . . 3 U H4' . 10018 1 14 . 1 1 4 4 U H5 H 1 5.788 0.02 . 1 . . . . 4 U H5 . 10018 1 15 . 1 1 4 4 U H6 H 1 7.925 0.02 . 1 . . . . 4 U H6 . 10018 1 16 . 1 1 4 4 U H1' H 1 5.537 0.02 . 1 . . . . 4 U H1' . 10018 1 17 . 1 1 4 4 U H2' H 1 4.401 0.02 . 1 . . . . 4 U H2' . 10018 1 18 . 1 1 5 5 G H8 H 1 7.763 0.02 . 1 . . . . 5 G H8 . 10018 1 19 . 1 1 5 5 G H1' H 1 5.656 0.02 . 1 . . . . 5 G H1' . 10018 1 20 . 1 1 5 5 G H2' H 1 4.64 0.02 . 1 . . . . 5 G H2' . 10018 1 21 . 1 1 5 5 G H3' H 1 4.311 0.02 . 1 . . . . 5 G H3' . 10018 1 22 . 1 1 5 5 G H4' H 1 4.42 0.02 . 1 . . . . 5 G H4' . 10018 1 23 . 1 1 6 6 U H5 H 1 5.411 0.02 . 1 . . . . 6 U H5 . 10018 1 24 . 1 1 6 6 U H6 H 1 7.608 0.02 . 1 . . . . 6 U H6 . 10018 1 25 . 1 1 6 6 U H1' H 1 5.25 0.02 . 1 . . . . 6 U H1' . 10018 1 26 . 1 1 6 6 U H2' H 1 3.95 0.02 . 1 . . . . 6 U H2' . 10018 1 27 . 1 1 6 6 U H3' H 1 4.5 0.02 . 1 . . . . 6 U H3' . 10018 1 28 . 1 1 6 6 U H4' H 1 4.328 0.02 . 1 . . . . 6 U H4' . 10018 1 29 . 1 1 7 7 A H2 H 1 6.986 0.02 . 1 . . . . 7 A H2 . 10018 1 30 . 1 1 7 7 A H8 H 1 8.308 0.02 . 1 . . . . 7 A H8 . 10018 1 31 . 1 1 7 7 A H1' H 1 5.945 0.02 . 1 . . . . 7 A H1' . 10018 1 32 . 1 1 7 7 A H2' H 1 4.656 0.02 . 1 . . . . 7 A H2' . 10018 1 33 . 1 1 7 7 A H3' H 1 4.765 0.02 . 1 . . . . 7 A H3' . 10018 1 34 . 1 1 7 7 A H4' H 1 4.494 0.02 . 1 . . . . 7 A H4' . 10018 1 35 . 1 1 8 8 C H5 H 1 5.942 0.02 . 1 . . . . 8 C H5 . 10018 1 36 . 1 1 8 8 C H6 H 1 7.831 0.02 . 1 . . . . 8 C H6 . 10018 1 37 . 1 1 8 8 C H1' H 1 5.911 0.02 . 1 . . . . 8 C H1' . 10018 1 38 . 1 1 8 8 C H2' H 1 4.454 0.02 . 1 . . . . 8 C H2' . 10018 1 39 . 1 1 8 8 C H3' H 1 4.609 0.02 . 1 . . . . 8 C H3' . 10018 1 40 . 1 1 9 9 G H8 H 1 7.482 0.02 . 1 . . . . 9 G H8 . 10018 1 41 . 1 1 9 9 G H1' H 1 5.598 0.02 . 1 . . . . 9 G H1' . 10018 1 42 . 1 1 9 9 G H2' H 1 4.864 0.02 . 1 . . . . 9 G H2' . 10018 1 43 . 1 1 9 9 G H3' H 1 4.102 0.02 . 1 . . . . 9 G H3' . 10018 1 44 . 1 1 9 9 G H4' H 1 4.488 0.02 . 1 . . . . 9 G H4' . 10018 1 45 . 1 1 10 10 U H5 H 1 5.039 0.02 . 1 . . . . 10 U H5 . 10018 1 46 . 1 1 10 10 U H6 H 1 7.533 0.02 . 1 . . . . 10 U H6 . 10018 1 47 . 1 1 10 10 U H1' H 1 5.451 0.02 . 1 . . . . 10 U H1' . 10018 1 48 . 1 1 10 10 U H2' H 1 4.183 0.02 . 1 . . . . 10 U H2' . 10018 1 49 . 1 1 10 10 U H3' H 1 4.471 0.02 . 1 . . . . 10 U H3' . 10018 1 50 . 1 1 10 10 U H4' H 1 4.373 0.02 . 1 . . . . 10 U H4' . 10018 1 51 . 1 1 11 11 C H5 H 1 5.779 0.02 . 1 . . . . 11 C H5 . 10018 1 52 . 1 1 11 11 C H6 H 1 7.975 0.02 . 1 . . . . 11 C H6 . 10018 1 53 . 1 1 11 11 C H1' H 1 5.728 0.02 . 1 . . . . 11 C H1' . 10018 1 54 . 1 1 11 11 C H2' H 1 4.553 0.02 . 1 . . . . 11 C H2' . 10018 1 55 . 1 1 11 11 C H3' H 1 4.629 0.02 . 1 . . . . 11 C H3' . 10018 1 56 . 1 1 11 11 C H4' H 1 4.374 0.02 . 1 . . . . 11 C H4' . 10018 1 57 . 1 1 12 12 G H8 H 1 7.616 0.02 . 1 . . . . 12 G H8 . 10018 1 58 . 1 1 12 12 G H1' H 1 5.698 0.02 . 1 . . . . 12 G H1' . 10018 1 59 . 1 1 12 12 G H2' H 1 4.586 0.02 . 1 . . . . 12 G H2' . 10018 1 60 . 1 1 12 12 G H3' H 1 4.437 0.02 . 1 . . . . 12 G H3' . 10018 1 61 . 1 1 12 12 G H4' H 1 4.508 0.02 . 1 . . . . 12 G H4' . 10018 1 62 . 1 1 13 13 C H5 H 1 5.181 0.02 . 1 . . . . 13 C H5 . 10018 1 63 . 1 1 13 13 C H6 H 1 7.735 0.02 . 1 . . . . 13 C H6 . 10018 1 64 . 1 1 13 13 C H1' H 1 5.524 0.02 . 1 . . . . 13 C H1' . 10018 1 65 . 1 1 13 13 C H2' H 1 4.431 0.02 . 1 . . . . 13 C H2' . 10018 1 66 . 1 1 14 14 U H5 H 1 5.408 0.02 . 1 . . . . 14 U H5 . 10018 1 67 . 1 1 14 14 U H6 H 1 7.895 0.02 . 1 . . . . 14 U H6 . 10018 1 68 . 1 1 14 14 U H1' H 1 5.523 0.02 . 1 . . . . 14 U H1' . 10018 1 69 . 1 1 14 14 U H2' H 1 4.421 0.02 . 1 . . . . 14 U H2' . 10018 1 70 . 1 1 15 15 U H5 H 1 5.582 0.02 . 1 . . . . 15 U H5 . 10018 1 71 . 1 1 15 15 U H6 H 1 7.988 0.02 . 1 . . . . 15 U H6 . 10018 1 72 . 1 1 15 15 U H1' H 1 5.631 0.02 . 1 . . . . 15 U H1' . 10018 1 73 . 1 1 15 15 U H2' H 1 4.245 0.02 . 1 . . . . 15 U H2' . 10018 1 74 . 1 1 15 15 U H3' H 1 4.556 0.02 . 1 . . . . 15 U H3' . 10018 1 75 . 1 1 16 16 U H5 H 1 5.376 0.02 . 1 . . . . 16 U H5 . 10018 1 76 . 1 1 16 16 U H6 H 1 7.633 0.02 . 1 . . . . 16 U H6 . 10018 1 77 . 1 1 16 16 U H1' H 1 5.632 0.02 . 1 . . . . 16 U H1' . 10018 1 78 . 1 1 16 16 U H2' H 1 4.31 0.02 . 1 . . . . 16 U H2' . 10018 1 79 . 1 1 16 16 U H3' H 1 4.423 0.02 . 1 . . . . 16 U H3' . 10018 1 80 . 1 1 16 16 U H4' H 1 4.353 0.02 . 1 . . . . 16 U H4' . 10018 1 81 . 1 1 17 17 G H8 H 1 7.664 0.02 . 1 . . . . 17 G H8 . 10018 1 82 . 1 1 17 17 G H1' H 1 5.445 0.02 . 1 . . . . 17 G H1' . 10018 1 83 . 1 1 17 17 G H2' H 1 4.357 0.02 . 1 . . . . 17 G H2' . 10018 1 84 . 1 1 17 17 G H3' H 1 4.663 0.02 . 1 . . . . 17 G H3' . 10018 1 85 . 1 1 18 18 G H8 H 1 7.663 0.02 . 1 . . . . 18 G H8 . 10018 1 86 . 1 1 18 18 G H1' H 1 5.341 0.02 . 1 . . . . 18 G H1' . 10018 1 87 . 1 1 18 18 G H2' H 1 4.385 0.02 . 1 . . . . 18 G H2' . 10018 1 88 . 1 1 18 18 G H3' H 1 4.414 0.02 . 1 . . . . 18 G H3' . 10018 1 89 . 1 1 18 18 G H4' H 1 4.045 0.02 . 1 . . . . 18 G H4' . 10018 1 90 . 1 1 19 19 A H2 H 1 7.917 0.02 . 1 . . . . 19 A H2 . 10018 1 91 . 1 1 19 19 A H8 H 1 8.097 0.02 . 1 . . . . 19 A H8 . 10018 1 92 . 1 1 19 19 A H1' H 1 5.856 0.02 . 1 . . . . 19 A H1' . 10018 1 93 . 1 1 19 19 A H2' H 1 4.671 0.02 . 1 . . . . 19 A H2' . 10018 1 94 . 1 1 19 19 A H3' H 1 4.739 0.02 . 1 . . . . 19 A H3' . 10018 1 95 . 1 1 19 19 A H4' H 1 4.384 0.02 . 1 . . . . 19 A H4' . 10018 1 96 . 1 1 20 20 U H5 H 1 5.825 0.02 . 1 . . . . 20 U H5 . 10018 1 97 . 1 1 20 20 U H6 H 1 7.804 0.02 . 1 . . . . 20 U H6 . 10018 1 98 . 1 1 20 20 U H1' H 1 5.914 0.02 . 1 . . . . 20 U H1' . 10018 1 99 . 1 1 20 20 U H2' H 1 4.407 0.02 . 1 . . . . 20 U H2' . 10018 1 100 . 1 1 20 20 U H3' H 1 4.693 0.02 . 1 . . . . 20 U H3' . 10018 1 101 . 1 1 20 20 U H4' H 1 4.466 0.02 . 1 . . . . 20 U H4' . 10018 1 102 . 1 1 20 20 U H5' H 1 4.194 0.02 . 1 . . . . 20 U H5' . 10018 1 103 . 1 1 21 21 A H2 H 1 7.956 0.02 . 1 . . . . 21 A H2 . 10018 1 104 . 1 1 21 21 A H8 H 1 7.925 0.02 . 1 . . . . 21 A H8 . 10018 1 105 . 1 1 21 21 A H1' H 1 5.834 0.02 . 1 . . . . 21 A H1' . 10018 1 106 . 1 1 21 21 A H2' H 1 4.869 0.02 . 1 . . . . 21 A H2' . 10018 1 107 . 1 1 21 21 A H3' H 1 4.555 0.02 . 1 . . . . 21 A H3' . 10018 1 108 . 1 1 22 22 A H2 H 1 7.131 0.02 . 1 . . . . 22 A H2 . 10018 1 109 . 1 1 22 22 A H8 H 1 7.896 0.02 . 1 . . . . 22 A H8 . 10018 1 110 . 1 1 22 22 A H1' H 1 4.98 0.02 . 1 . . . . 22 A H1' . 10018 1 111 . 1 1 22 22 A H2' H 1 4.516 0.02 . 1 . . . . 22 A H2' . 10018 1 112 . 1 1 22 22 A H3' H 1 4.46 0.02 . 1 . . . . 22 A H3' . 10018 1 113 . 1 1 23 23 A H2 H 1 7.12 0.02 . 1 . . . . 23 A H2 . 10018 1 114 . 1 1 23 23 A H8 H 1 7.593 0.02 . 1 . . . . 23 A H8 . 10018 1 115 . 1 1 23 23 A H1' H 1 5.771 0.02 . 1 . . . . 23 A H1' . 10018 1 116 . 1 1 23 23 A H2' H 1 4.474 0.02 . 1 . . . . 23 A H2' . 10018 1 117 . 1 1 24 24 A H2 H 1 7.367 0.02 . 1 . . . . 24 A H2 . 10018 1 118 . 1 1 24 24 A H8 H 1 7.65 0.02 . 1 . . . . 24 A H8 . 10018 1 119 . 1 1 24 24 A H1' H 1 5.82 0.02 . 1 . . . . 24 A H1' . 10018 1 120 . 1 1 24 24 A H2' H 1 4.514 0.02 . 1 . . . . 24 A H2' . 10018 1 121 . 1 1 24 24 A H3' H 1 4.573 0.02 . 1 . . . . 24 A H3' . 10018 1 122 . 1 1 25 25 G H8 H 1 7.083 0.02 . 1 . . . . 25 G H8 . 10018 1 123 . 1 1 25 25 G H1' H 1 5.528 0.02 . 1 . . . . 25 G H1' . 10018 1 124 . 1 1 25 25 G H2' H 1 4.327 0.02 . 1 . . . . 25 G H2' . 10018 1 125 . 1 1 26 26 C H5 H 1 5.051 0.02 . 1 . . . . 26 C H5 . 10018 1 126 . 1 1 26 26 C H6 H 1 7.461 0.02 . 1 . . . . 26 C H6 . 10018 1 127 . 1 1 26 26 C H1' H 1 5.476 0.02 . 1 . . . . 26 C H1' . 10018 1 128 . 1 1 26 26 C H2' H 1 4.627 0.02 . 1 . . . . 26 C H2' . 10018 1 129 . 1 1 26 26 C H3' H 1 4.424 0.02 . 1 . . . . 26 C H3' . 10018 1 130 . 1 1 26 26 C H4' H 1 4.333 0.02 . 1 . . . . 26 C H4' . 10018 1 131 . 1 1 27 27 G H8 H 1 7.409 0.02 . 1 . . . . 27 G H8 . 10018 1 132 . 1 1 27 27 G H1' H 1 5.674 0.02 . 1 . . . . 27 G H1' . 10018 1 133 . 1 1 27 27 G H2' H 1 4.575 0.02 . 1 . . . . 27 G H2' . 10018 1 134 . 1 1 27 27 G H3' H 1 4.184 0.02 . 1 . . . . 27 G H3' . 10018 1 135 . 1 1 27 27 G H4' H 1 4.475 0.02 . 1 . . . . 27 G H4' . 10018 1 136 . 1 1 28 28 U H5 H 1 5.138 0.02 . 1 . . . . 28 U H5 . 10018 1 137 . 1 1 28 28 U H6 H 1 7.532 0.02 . 1 . . . . 28 U H6 . 10018 1 138 . 1 1 28 28 U H1' H 1 5.414 0.02 . 1 . . . . 28 U H1' . 10018 1 139 . 1 1 28 28 U H2' H 1 4.218 0.02 . 1 . . . . 28 U H2' . 10018 1 140 . 1 1 28 28 U H3' H 1 4.391 0.02 . 1 . . . . 28 U H3' . 10018 1 141 . 1 1 28 28 U H4' H 1 4.364 0.02 . 1 . . . . 28 U H4' . 10018 1 142 . 1 1 29 29 C H5 H 1 5.698 0.02 . 1 . . . . 29 C H5 . 10018 1 143 . 1 1 29 29 C H6 H 1 7.984 0.02 . 1 . . . . 29 C H6 . 10018 1 144 . 1 1 29 29 C H1' H 1 5.612 0.02 . 1 . . . . 29 C H1' . 10018 1 145 . 1 1 29 29 C H2' H 1 4.378 0.02 . 1 . . . . 29 C H2' . 10018 1 146 . 1 1 29 29 C H3' H 1 4.468 0.02 . 1 . . . . 29 C H3' . 10018 1 147 . 1 1 30 30 U H5 H 1 5.555 0.02 . 1 . . . . 30 U H5 . 10018 1 148 . 1 1 30 30 U H6 H 1 7.963 0.02 . 1 . . . . 30 U H6 . 10018 1 149 . 1 1 30 30 U H1' H 1 5.585 0.02 . 1 . . . . 30 U H1' . 10018 1 150 . 1 1 30 30 U H2' H 1 4.548 0.02 . 1 . . . . 30 U H2' . 10018 1 151 . 1 1 30 30 U H3' H 1 4.607 0.02 . 1 . . . . 30 U H3' . 10018 1 152 . 1 1 30 30 U H4' H 1 4.436 0.02 . 1 . . . . 30 U H4' . 10018 1 153 . 1 1 31 31 G H8 H 1 7.786 0.02 . 1 . . . . 31 G H8 . 10018 1 154 . 1 1 31 31 G H1' H 1 5.808 0.02 . 1 . . . . 31 G H1' . 10018 1 155 . 1 1 31 31 G H2' H 1 4.47 0.02 . 1 . . . . 31 G H2' . 10018 1 156 . 1 1 31 31 G H3' H 1 4.543 0.02 . 1 . . . . 31 G H3' . 10018 1 157 . 1 1 32 32 C H5 H 1 5.397 0.02 . 1 . . . . 32 C H5 . 10018 1 158 . 1 1 32 32 C H6 H 1 7.586 0.02 . 1 . . . . 32 C H6 . 10018 1 159 . 1 1 32 32 C H1' H 1 5.419 0.02 . 1 . . . . 32 C H1' . 10018 1 160 . 1 1 32 32 C H2' H 1 4.316 0.02 . 1 . . . . 32 C H2' . 10018 1 161 . 1 1 32 32 C H3' H 1 4.481 0.02 . 1 . . . . 32 C H3' . 10018 1 162 . 1 1 33 33 G H8 H 1 7.383 0.02 . 1 . . . . 33 G H8 . 10018 1 163 . 1 1 33 33 G H1' H 1 5.613 0.02 . 1 . . . . 33 G H1' . 10018 1 164 . 1 1 33 33 G H2' H 1 4.747 0.02 . 1 . . . . 33 G H2' . 10018 1 165 . 1 1 34 34 A H2 H 1 7.862 0.02 . 1 . . . . 34 A H2 . 10018 1 166 . 1 1 34 34 A H8 H 1 7.884 0.02 . 1 . . . . 34 A H8 . 10018 1 167 . 1 1 34 34 A H1' H 1 5.914 0.02 . 1 . . . . 34 A H1' . 10018 1 168 . 1 1 34 34 A H2' H 1 4.454 0.02 . 1 . . . . 34 A H2' . 10018 1 169 . 1 1 35 35 C H5 H 1 5.146 0.02 . 1 . . . . 35 C H5 . 10018 1 170 . 1 1 35 35 C H6 H 1 7.478 0.02 . 1 . . . . 35 C H6 . 10018 1 171 . 1 1 35 35 C H1' H 1 5.41 0.02 . 1 . . . . 35 C H1' . 10018 1 172 . 1 1 35 35 C H2' H 1 4.117 0.02 . 1 . . . . 35 C H2' . 10018 1 173 . 1 1 35 35 C H4' H 1 4.351 0.02 . 1 . . . . 35 C H4' . 10018 1 174 . 1 1 36 36 C H5 H 1 5.395 0.02 . 1 . . . . 36 C H5 . 10018 1 175 . 1 1 36 36 C H6 H 1 7.626 0.02 . 1 . . . . 36 C H6 . 10018 1 176 . 1 1 36 36 C H1' H 1 5.747 0.02 . 1 . . . . 36 C H1' . 10018 1 177 . 1 1 36 36 C H2' H 1 3.985 0.02 . 1 . . . . 36 C H2' . 10018 1 178 . 1 1 36 36 C H3' H 1 4.14 0.02 . 1 . . . . 36 C H3' . 10018 1 stop_ save_