# 1 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" ;mlevph ;avance-version (10/01/28) ;homonuclear Hartman-Hahn transfer using MLEV17 sequence ; for mixing ;using two power levels for excitation and spinlock ;phase sensitive ; ;A. Bax & D.G. Davis, J. Magn. Reson. 65, 355-360 (1985) ; ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= # 1 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance3.incl ; for AV III ; ;avance-version (07/12/14) ; ;$CLASS=HighRes Incl ;$COMMENT= # 165 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Avance.incl" ;$Id: Avance3.incl,v 1.9 2009/07/02 16:40:43 ber Exp $ # 17 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" 2 # 1 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Delay.incl" 1 ;Delay.incl - include file for commonly used delays ; ;version 00/02/07 ; ;$CLASS=HighRes Incl ;$COMMENT= # 9 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Delay.incl" ;general delays define delay DELTA define delay DELTA1 define delay DELTA2 define delay DELTA3 define delay DELTA4 define delay DELTA5 define delay DELTA6 define delay DELTA7 define delay DELTA8 define delay TAU define delay TAU1 define delay TAU2 define delay TAU3 define delay TAU4 define delay TAU5 # 29 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Delay.incl" ;delays for centering pulses define delay CEN_HN1 define delay CEN_HN2 define delay CEN_HN3 define delay CEN_HC1 define delay CEN_HC2 define delay CEN_HC3 define delay CEN_HC4 define delay CEN_HP1 define delay CEN_HP2 define delay CEN_CN1 define delay CEN_CN2 define delay CEN_CN3 define delay CEN_CN4 define delay CEN_CP1 define delay CEN_CP2 # 48 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Delay.incl" ;loop counters define loopcounter COUNTER define loopcounter SCALEF define loopcounter FACTOR1 define loopcounter FACTOR2 define loopcounter FACTOR3 # 58 "/opt/topspin3.0/exp/stan/nmr/lists/pp/Delay.incl" ;$Id: Delay.incl,v 1.13 2009/07/02 16:40:43 ber Exp $ # 18 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" 2 # 21 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" "p5=p6*.667" "p7=p6*2" "d12=20u" "in0=inf1" # 28 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" "d0=in0/2-p1*2/3.1416-4u" "SCALEF=p7*2/p5" "FACTOR1=((d9-p17*2)/(p6*64+p5))/SCALEF" "l1=FACTOR1*SCALEF" # 1 "mc_line 36 file /opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph exp. def. part of mc cmd. before ze" define delay MCWRK define delay MCREST define delay d0orig "d0orig=d0" define loopcounter t1loop "t1loop=0" define loopcounter ph1loop "ph1loop=0" define loopcounter ST1CNT "ST1CNT = td1/(2)" "MCWRK = 0.200000*d1" "MCREST = d1 - d1" dccorr # 36 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" # 36 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" 1 ze # 1 "mc_line 36 file /opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph exp. def. of mc cmd. after ze" # 37 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" # 1 "mc_line 37 file /opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph exp. start label for mc cmd." 2 MCWRK * 2 LBLF1, MCWRK * 2 LBLST1, MCWRK MCREST # 38 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" 3 d12 pl1:f1 p1 ph1 d0 4u pl10:f1 (p17 ph26) ;begin MLEV17 4 (p6 ph22 p7 ph23 p6 ph22) (p6 ph24 p7 ph25 p6 ph24) (p6 ph24 p7 ph25 p6 ph24) (p6 ph22 p7 ph23 p6 ph22) (p6 ph24 p7 ph25 p6 ph24) (p6 ph24 p7 ph25 p6 ph24) (p6 ph22 p7 ph23 p6 ph22) (p6 ph22 p7 ph23 p6 ph22) (p6 ph24 p7 ph25 p6 ph24) (p6 ph22 p7 ph23 p6 ph22) (p6 ph22 p7 ph23 p6 ph22) (p6 ph24 p7 ph25 p6 ph24) (p6 ph22 p7 ph23 p6 ph22) (p6 ph22 p7 ph23 p6 ph22) (p6 ph24 p7 ph25 p6 ph24) (p6 ph24 p7 ph25 p6 ph24) (p5 ph23) lo to 4 times l1 ;end MLEV17 (p17 ph26) go=2 ph31 # 1 "mc_line 65 file /opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph exp. mc cmd. in line" MCWRK wr #0 if #0 zd "ph1loop+=1" "d0=d0orig + t1loop * in0 " "phval1 = (ph1loop % 4) * 90" MCWRK ip1 + phval1 lo to LBLF1 times 2 MCWRK "t1loop+=1" "d0=d0orig + t1loop * in0 " "phval1 = (ph1loop % 4) * 90" MCWRK ip1 + phval1 lo to LBLST1 times ST1CNT MCWRK "t1loop=0" "ph1loop=0" MCWRK # 66 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" exit ph1=0 2 2 0 1 3 3 1 ph22=3 1 3 1 0 2 0 2 ph23=0 2 0 2 1 3 1 3 ph24=1 3 1 3 2 0 2 0 ph25=2 0 2 0 3 1 3 1 ph26=0 2 0 2 1 3 1 3 ph31=0 2 2 0 1 3 3 1 # 78 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" ;pl1 : f1 channel - power level for pulse (default) ;pl10: f1 channel - power level for TOCSY-spinlock ;p1 : f1 channel - 90 degree high power pulse ;p5 : f1 channel - 60 degree low power pulse ;p6 : f1 channel - 90 degree low power pulse ;p7 : f1 channel - 180 degree low power pulse ;p17: f1 channel - trim pulse [2.5 msec] ;d0 : incremented delay (2D) ;d1 : relaxation delay; 1-5 * T1 ;d9 : TOCSY mixing time ;d12: delay for power switching [20 usec] ;l1: loop for MLEV cycle: (((p6*64) + p5) * l1) + (p17*2) = mixing time ;inf1: 1/SW = 2 * DW ;in0: 1/(1 * SW) = 2 * DW ;nd0: 1 ;NS: 8 * n ;DS: 16 ;td1: number of experiments ;FnMODE: States-TPPI, TPPI, States or QSEQ ;Processing # 101 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" ;PHC0(F1): 180 ;PHC1(F1): -180 ;FCOR(F1): 1 # 107 "/opt/topspin3.0/exp/stan/nmr/lists/pp/mlevph" ;$Id: mlevph,v 1.10.2.1 2010/02/02 15:31:39 ber Exp $