NMRbot_cq_sphingomyelin_SampleReport.20140514_1446.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## NMRbot version 20140226 ## ## Initiated - 20140514_1446 ## - info: cq_sphingomyelin in MMCD_mixed at position 202 foldername => cq_sphingomyelin.MMCD_mixed.202.20140514 Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 202 - passed - MMCD_mixed solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - creating exp 1 with ZGCPPR parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 40.3 - creating exp 2 with metabTOCSY parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 101 - creating exp 3 with C13CPD parameters - prosol parameters loaded - NS changed to 2048 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - prosol parameters loaded - NS changed to 4 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - prosol parameters loaded - NS changed to 4 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND parameters - prosol parameters loaded - NS changed to 8 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 45.2 - creating exp 10 with HSQC_TOCSY_ADIA parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.03 - start 20140514_1457 - end 20140514_1458 - passed - 1H adaptive offset determined = 4.7498 - 1H adaptive SW determined = 16.7513 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21 - start 20140514_1458 - end 20140514_1736 - passed # Exp 3 - C13CPD (zgpg30) - dims 1- F1 13C, SW 236.77 - start 20140514_1736 - end 20140514_1924 - passed # Exp 4 - C13DEPT90 (deptsp90) - dims 1- F1 13C, SW 236.77 - start 20140514_1924 - end 20140514_1951 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.77 - start 20140514_1951 - end 20140514_2018 - passed - 13C adaptive offset determined = 74.1601 - 13C adaptive SW determined = 130.5538 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99 - start 20140514_2018 - end 20140514_2046 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - F1 SW changed to 130.55 - F2 SW changed to 16.75 - F1 1H offset changed to 4.75 - F2 13C offset changed to 74.16 - dims 2- F1 13C, SW 130.55; F2 1H, SW 16.75 - start 20140514_2046 - end 20140514_2114 - passed # Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd) - dims 2- F1 13C, SW 221.83; F2 1H, SW 12.02 - start 20140514_2114 - end 20140514_2237 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31 - start 20140514_2237 - end 20140514_2353 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02 - start 20140514_2353 - end 20140515_0229 - passed ## cq_sphingomyelin Experiment Set Ended - 20140515_0229 ##