NMRbot_CAS_186800-61-3_SampleReport.20140515_0229.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20140515_0229 ##

- info:
  CAS_186800-61-3 in MMCD_mixed at position 203
  foldername => CAS_186800-61-3.MMCD_mixed.203.20140514
  Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 203 - passed
- MMCD_mixed solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 114
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 3 with C13CPD parameters
-   prosol parameters loaded
-   NS changed to 2048
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   NS changed to 512
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   NS changed to 512
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 4
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 4
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 128
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20140515_0240
- end   20140515_0241 - passed
-   1H adaptive offset determined = 4.7498
-   1H adaptive SW determined = 17.0285
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20140515_0241
- end   20140515_0518 - passed
# Exp 3 - C13CPD (zgpg30)
- dims 1- F1 13C, SW 236.77
- start 20140515_0518
- end   20140515_0707 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20140515_0707
- end   20140515_0734 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20140515_0734
- end   20140515_0801 - passed
-   13C adaptive offset determined = 39.1812
-   13C adaptive SW determined = 86.7099
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99
- start 20140515_0801
- end   20140515_0829 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 86.71
-   F2 SW changed to 17.03
-   F1 1H offset changed to 4.75
-   F2 13C offset changed to 39.18
- dims 2- F1 13C, SW 86.71; F2 1H, SW 17.01
- start 20140515_0829
- end   20140515_0857 - passed
# Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd)
- dims 2- F1 13C, SW 221.83; F2 1H, SW 12.02
- start 20140515_0857
- end   20140515_1020 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31
- start 20140515_1020
- end   20140515_1136 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02
- start 20140515_1136
- end   20140515_1412 - passed

## CAS_186800-61-3 Experiment Set Ended - 20140515_1412 ##