BMRB

Biological Magnetic Resonance Data Bank


A Repository for Data from NMR Spectroscopy on Proteins, Peptides, Nucleic Acids, and other Biomolecules
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DL-beta-leucine (C6 H13 N O2)

Natural Isotopic formula weight: 131.17292

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bmse000466 Data

Entry STAR file: bmse000466.str
NMR-STAR interactive viewer
Time Domain Data: bmse000466.zip
BMRB Entry DOI: doi:10.13018/BMSE000466
Mol file: bmse000466.mol

DL-beta-leucine
Source:   sigma
Solvent:   100 % D2O
Buffer:   50 mM sodium phosphate
Cytocide:   500 µM sodium azide
Reference:   500 µM DSS

Concentration and pH are given with spectrum
Spectrometer: Bruker DMX - 500 MHz

Data Source: Madison Metabolomics Consortium - Qiu Cui, Ian Lewis, Francisca Jofre, Mark E. Anderson, John L. Markley.

View the GISSMO record for this entry.

Atom numbering calculated using ALATIS. Citation: Hesam Dashti, William M. Westler, John L. Markley, Hamid R. Eghbalnia, "Unique identifiers for small molecules enable rigorous labeling of their atoms", Scientific Data 4, Article number: 170073 (2017), doi:10.1038/sdata.2017.73, https://www.nature.com/articles/sdata201773

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Experimental Data:

1D 1H

Concentration: 100 mM
temperature: 298 K
pH: 7.4
1D 1H, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_1.zip
View Spectral peak list

2D [1H,1H]-TOCSY

Concentration: 100 mM
temperature: 298 K
pH: 7.4
2D [1H,1H]-TOCSY, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_2.zip

1D 13C

Concentration: 100 mM
temperature: 298 K
pH: 7.4
1D 13C, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_3.zip
View Spectral peak list

1D DEPT90

Concentration: 100 mM
temperature: 298 K
pH: 7.4
1D DEPT90, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_4.zip
View Spectral peak list

1D DEPT135

Concentration: 100 mM
temperature: 298 K
pH: 7.4
1D DEPT135, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_5.zip
View Spectral peak list

2D [1H,13C]-HSQC

Concentration: 100 mM
temperature: 298 K
pH: 7.4
2D [1H,13C]-HSQC, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_6.zip
View Spectral peak list

2D [1H,13C]-HMBC

Concentration: 100 mM
temperature: 298 K
pH: 7.4
2D [1H,13C]-HMBC, 7.4 spectrum for DL-beta-leucine
Download data directory: bmse000466_7.zip