D-Glucosamine 6-phosphate (C6H14NO8P)
BMRB entry bmse000189
Entry DOI: doi:10.13018/BMSE000189
Data source: Madison Metabolomics Consortium - Qiu Cui, Ian Lewis, Gareth Westler, Mark E. Anderson, John L. Markley
NMR-STAR file:
bmse000189.strNMR-STAR
interactive viewerStructure file (mol/sdf):
bmse000189.molAll files for
bmse000189Time Domain Data:
bmse000189.zipSample and instrument details are given with the spectrum
Assigned chemical shifts
Set 1
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
| Atom ID | Author Nomenclature | Value | Ambiguity Code |
|---|---|---|---|
| C6 | C1 | 96.285 | 6 |
| C3 | C2 | 59.752 | 6 |
| C5 | C3 | 71.968 | 6 |
| C4 | C4 | 74.837 | 6 |
| C2 | C5 | 78.382 | 6 |
| C1 | C6 | 65.413 | 6 |
| H23 | H17 | 5.458 | 6 |
| H20 | H18 | 3.291 | 6 |
| H22 | H19 | 3.879 | 6 |
| H21 | H20 | 3.656 | 6 |
| H19 | H21 | 3.937 | 6 |
| H17 | H22 | 4.008 | 6 |
| H18 | H23 | 4.001 | 6 |
NMR experiments
1: 1D 1H
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
2: 2D [1H,1H]-TOCSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
3: 1D 13C
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
4: 1D DEPT90
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
5: 1D DEPT135
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
6: 2D [1H,13C]-HSQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
