;hmqcnoejr1d.wmw ;MANUFACTURER: Bruker ;MODEL: NMRFAM DMX 750 ;DESCRIPTION: 13C edited (HMQC) 1D NOE difference ;JR for water suppression (9/27/94) ;W. M. Westler ;BMRB Pulse Sequence Accession Number: 16 #include #include 1 ze 2 d1 do:f2 LOCKH_OFF ;lock hold off 30u LOCKH_ON ;lock hold on 3 (p1 ph1):f1 ;90 degree pulse 1H at pl1 d2 pl2:f2 ;1/2JCH pl2 pulse level for 13C p3:f2 ph3 (p1*2 ph2):f1 p3:f2 ph4 d2 pl12:f2 ;pl12 13C decoupling power level (p1 ph5):f1 GRADIENT(cnst22) ;crusher gradient (delay radiation damp) d9 (p1 ph6):f1 ;jump-return read pulse (on resonance H2O) d4 (p4 ph7):f1 ;p4 adjusted to reduce h2o (nominal 90) go=2 ph31 cpd2:f2 d1 do:f2 wr #0 30u LOCKH_OFF exit ph1=0 ph2=0 ph3=0 2 ph4=0 0 2 2 ph5= 0 0 0 0 ph6= 0 0 0 0 ph7= 2 2 2 2 ph31=0 2 2 0 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;pl12: f2 channel - power level for CPD/BB decoupling ;p1 : f1 channel - 90 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p4 : f1 channel - adjustable flip back pulse for water (nominal 90) ;p31: - 90 degree pulse for decoupling sequence ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J)XH ;NS: 4 * n ;DS: 8-16 ;cpd2: decoupling according to sequence defined by cpdprg2