;hsqclr.abx hsqc with selective 180(1H) pulses for high S/N ;J. Magn. Reson. Ser A 119, 134-138 (1996), figure 1C. ;long-range correlation. Process phase sensitive (States mode on Bruke r) ;low power GARP during data acq. (gB2 = 13C(SW)/5 for dl0). ;fully decoupled in 13C dimension ;carefully adjust ph0 to be the same phase as ph1 to minimize t1 noise ;BMRB Pulse Sequence Accession Number: 8 #include "bits.sg" ;home made gradient pulse control d12=7m d4=40m d26=p2-p3*2.2 d11=50m 1 ze 10u CLEAR_BITS ;reset all external control lines 2 d11 do 3 d12*2 4 1m do d1 RESET ;reset all external control lines, lock on 1m dhi hl1 HIGH(11) ;lock hold on p1 ph1 2u GRAD(20, POSITIV, 10) ;500 us gradient d5 hl2 (p2*2 ph0):f1 (d26 p3 ph2 2u p3*2.4 ph12 2u p3 ph2):f2 2u GRAD(21, POSITIV, 10) ;500 us gradient d5 hl1 (p1 ph10):f1 GRAD(22, POSITIV, 60) ;3 ms gradient (p3 ph3):f2 d0 p1*2 ph0 d0 (p3 ph2):f2 (p1 ph1):f1 2u GRAD(30, POSITIV, 6) ;300 us gradient d4 hl2 (p2*2 ph0):f1 (d26 p3 ph2 2u p3*2.4 ph12 2u p3 ph2):f2 2u GRAD(31, POSITIV, 6) ;300 us gradient d4 hl1 dlo (p1 ph30):f1 2u dl0 go=2 ph31 cpd d11 do wr #0 if #0 ip3 zd lo to 3 times 2 d12 ip31 lo to 3 times l3 1m RESET do exit ph1=0 ph31=0 2 2 0 ph0=(360)325 ph3=0 0 2 2 ph2=0 ph12=1 ph10=1 3 ph30=0